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US4992298A Expired / Lapsed US ⏱️ 0.0 years remaining

Dual ion beam ballistic alloying process

Assignee: BEAMALLOY TECHNOLOGIES LLC
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Filing: 1988-10-11
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Granted: 1991-02-12
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Expires: 2008-10-11
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Abstract

Abstract The invention discloses a dual ion beam ballistic alloying process for forming a film such as diamond onto a substrate, which comprises the steps of: (a) cleaning the surface of the substrate with a first energy beam of inert atoms; (b) depositing a layer of a desired non-hydrocarbon substance on the substrate with a low energy, sputtered atomic beam; (c) simultaneously exposing the substrate to said first energy beam of inert atoms with a high energy to grow a ballistically alloyed layer having a thickness of about 10-2000 Å; and (d) reducing the energy level of the first, high energy beam to cause the growth of the layer of said substance on said substrate to a final desired thickness.

Inventors

  • 👤 Arnold H. Deutchman
  • 👤 Robert J. Partyka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 02:23
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; B; B29; B29D; B29D11/00; B29D11/00009; C23C14/02; C23C14/021; C23C14/022; B29C; B29C33/00; B29C33/56; B29K; B29K2105/00; B29K2105/06; Y; Y10; Y10S; Y10S427/00; Y10S427/103; Y10S427/105; Y10S505/00; Y10S505/80; Y10S505/815; Y10S505/818

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 200 words
A process for forming a film adhered to a substrate in an evacuated atmosphere comprising: (a) cleaning the surface of the substrate with a first energy beam of inert atoms having an energy level in the range from about 500 eV to 1000 eV, (b) after said cleaning, sputtering a desired non-hydrocarbon substance within said atmosphere by a second beam of inert atoms having an energy rate of about 1-50 eV/atom at a rate and in a direction to cause such substance to deposit on said substrate, (c) simultaneously with said sputtering, exposing the substrate to said first energy beam of inert atoms at an energy level in the range from about 0.5 KeV to 100 KeV to grow a ballistically alloyed layer having a thickness of about 10-2000Å in said substrate, (d) subsequently of exposing the substrate to the first beam and the sputtering, continuing the sputtering and exposing the substrate to a lower energy beam of inert atoms from the source of said first beam at an energy level in the range from about 100 eV to 500 eV that will cause the growth of a film of said substance on said substrate to a final desired thickness.
Claim 2
Dependent Claim 200 words
A process for forming a film adhered to a substrate in an evacuated atmosphere comprising: (a) cleaning the surface of the substrate with a first energy beam of inert atoms having an energy level in the range from about 500 eV to 1000 eV, (b) after said cleaning, sputtering a desired non-hydrocarbon substance within said atmosphere by a second beam of inert atoms having an energy rate of about 1-50 eV/atom at a rate and in a direction to cause such substance to deposit on said substrate, (c) simultaneously with said sputtering, exposing the substrate to said first energy beam of inert atoms at an energy level in the range from about 0.5 KeV to 100 KeV to grow a ballistically alloyed layer having a thickness of about 10-2000Å in said substrate, (d) subsequently of exposing the substrate to the first beam and the sputtering, continuing the sputtering and exposing the substrate to a lower energy beam of inert atoms from the source of said first beam at an energy level in the range from about 100 eV to 500 eV that will cause the growth of a film of said substance on said substrate to a final desired thickness.
Claim 3
Dependent Claim 20 words
A process according to claim 1 wherein the film is selected from diamond, nitrides, borides, carbides, oxides and diamond-like films.
Claim 4
Dependent Claim 11 words
A process according to claim 2 wherein the film is diamond.
Claim 5
Dependent Claim 30 words
A process according to claim 1 wherein the temperature in the evacuated atmosphere is less than about 300° F. and the pressure ranges from about 10 -3 -10 -6 torr.
Claim 6
Dependent Claim 17 words
A process according to claim 1 wherein the substrate is selected from metals, ceramics, glasses and plastics.
Claim 7
Dependent Claim 27 words
A process according to claim 1 wherein the first energy beam is selected from atoms of argon, neon, krypton, and xenon at the beginning of said sputtering.
Claim 8
Dependent Claim 25 words
A process according to claim 1 wherein the sputtered ion beam is selected from atoms of graphite, boron, silicon, metals, refractory carbides, nitrides or oxides.
Claim 9
Dependent Claim 19 words
A process according to claim 1 wherein the ballistically alloyed layer has a thickness ranging from about 10-20 Å.
Claim 10
Dependent Claim 20 words
A process according to claim 1 wherein the film is deposited at a rate of about 0.1 to 10 Å/min.
Claim 11
Dependent Claim 15 words
The process of claim 1 wherein the process is conducted in the absence of hydrogen.
Claim 12
Dependent Claim 15 words
The process of claim 2 wherein the process is conducted in the absence of hydrogen.
Claim 13
Dependent Claim 15 words
The process of claim 4 wherein the process is conducted in the absence of hydrogen.
Claim 14
Dependent Claim 15 words
The process of claim 5 wherein the process is conducted in the absence of hydrogen.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1994-02-11 1994-08-13 1995-02-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1998-02-11 1998-08-13 1999-02-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2002-02-11 2002-08-13 2003-02-12 $7700.00 Window Closed / Lapsed

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