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US4859383A Expired / Lapsed US ⏱️ 0.0 years remaining

Process of producing a composite macrostructure of organic and inorganic materials

Assignee: Bio Medical Sciences Inc
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Filing: 1988-04-25
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Granted: 1989-08-22
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Expires: 2008-04-25
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Abstract

Abstract A composite self-supporting flexible agglomerated macrostructure is described which includes (1) a matrix of unfibrillated polytetrafluoroethylene resin and addition curable silicone and (2) particulate material including hydroxyapatite and/or tricalcium phosphate uniformly distributed throughout said matrix, the macrostructure being uniformly permeated by a network of open pores formed in the process of manufacture by intimately blending particulate sodium chloride and subsequently leaching the sodium chloride particles.

Inventors

  • 👤 Mark E. Dillon

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 06:59
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/26; A; A61; A61L; A61L27/00; A61L27/40; A61L27/44; A61L27/46; C04; C04B; C04B26/00; C04B26/30; C04B26/32; C08K; C08K3/00; C08K3/32; C08J2327/00; C08J2327/02; C08J2327/12; C08J2327/18

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 185 words
A process of producing a composite macrostructure comprising the steps of first (1) intimately blending a mixture of a major amount of unsintered and unfibrillated particulate polytetrafluoroethylene resin and minor amounts of (A) a hydrocarbon liquid and (B) an addition curable silicone composition containing a crosslinking catalyst, then (2) intimately blending with the product of step (1) both a particulate ceramic material selected from the group consisting of hydroxyapatite and tricalcium phosphate and a particulate sodium chloride whose particle size is determined by a desired size of open pores in the macrostructure, then (3) introducing the product of step (2) into opposing streams of air within a mill so as to form a homogeneous particulate mixture, then (4) subjecting the product of step (3) to mechanical pressure within a die, then (5) hot pressing the product of step (4) at a temperature sufficient to sinter the polytetrafluoroethylene and to cure the silicone composition and then (6) solubilizing the particulate sodium chloride so as to create a network of open pores in the product of step (6) corresponding in size to the original sodium chloride particles.
Claim 2
Dependent Claim 185 words
A process of producing a composite macrostructure comprising the steps of first (1) intimately blending a mixture of a major amount of unsintered and unfibrillated particulate polytetrafluoroethylene resin and minor amounts of (A) a hydrocarbon liquid and (B) an addition curable silicone composition containing a crosslinking catalyst, then (2) intimately blending with the product of step (1) both a particulate ceramic material selected from the group consisting of hydroxyapatite and tricalcium phosphate and a particulate sodium chloride whose particle size is determined by a desired size of open pores in the macrostructure, then (3) introducing the product of step (2) into opposing streams of air within a mill so as to form a homogeneous particulate mixture, then (4) subjecting the product of step (3) to mechanical pressure within a die, then (5) hot pressing the product of step (4) at a temperature sufficient to sinter the polytetrafluoroethylene and to cure the silicone composition and then (6) solubilizing the particulate sodium chloride so as to create a network of open pores in the product of step (6) corresponding in size to the original sodium chloride particles.
Claim 3
Dependent Claim 15 words
The process of claim 1, wherein the pressure of step (4) is about 5,000 psi.
Claim 4
Dependent Claim 14 words
The process of claim 1, wherein the pressure of step (5) is 2,000 psi.
Claim 5
Dependent Claim 14 words
The process of claim 1, wherein the temperature of step (5) is 340° C.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1992-08-21 1993-02-20 1993-08-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1996-08-21 1997-02-20 1997-08-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2000-08-21 2001-02-20 2001-08-22 $7700.00 Window Closed / Lapsed

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