US4704126A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Chemical polishing process for titanium and titanium alloy surgical implants
Assignee: NEC Corp
•
Filing: 1985-04-15
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Granted: 1987-11-03
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Expires: 2005-04-15
Abstract
Abstract A method of chemically polishing medical implants by immersing them in a solution including lactic acid, hydrofluoric acid, and nitric acid to produce smooth, matte finished implants.
Inventors
- 👤 Imogene Baswell
- 👤 Kimberly Walsh
- 👤 Eric Benz
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 03:53
CPC Classifications
A; A61; A61F; A61F2/00; A61F2/02; A61F2/30; A61F2/30767; A61F11/00; A61F11/20; A61F11/202; C; C23; C23F; C23F3/00; C23F3/04; C23F3/06
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
79 words
A method of polishing a surgical ear tube implant formed of a biocompatible titanium or titanium alloy having a smooth polished surface that discourages tissue growth thereon, comprising the steps of: a. contacting the implant with a polishing solution including lactic acid, hydrofluoric acid and nitric acid; b. moving the implant and polishing compound relative one to the other; and thereafter c. washing the implant to remove substantially all of the polishing compound until the alloy has matte finish.
Claim 2
Independent Claim
79 words
A method of polishing a surgical ear tube implant formed of a biocompatible titanium or titanium alloy having a smooth polished surface that discourages tissue growth thereon, comprising the steps of: a. contacting the implant with a polishing solution including lactic acid, hydrofluoric acid and nitric acid; b. moving the implant and polishing compound relative one to the other; and thereafter c. washing the implant to remove substantially all of the polishing compound until the alloy has matte finish.
Claim 3
Dependent Claim
50 words
The method of claim 1 wherein the contacting step includes immersing the implant in a polishing solution that comprises: from about 60 to about 79 weight percent lactic acid; from about 10.5 to about 20 weight percent hydroflouric acid; and from about 10.5 to about 20 weight percent nitric acid.
Claim 4
Dependent Claim
17 words
The method of claim 1, wherein the moving step includes agitating the immersed implant in the solution.
Claim 5
Dependent Claim
32 words
The method of claim 1 wherein the contacting and moving steps are carried out long enough to effectively remove surface irregularities on the implant without removing excessive amounts of the implant material.
Claim 6
Dependent Claim
39 words
The method of claim 3 wherein the washing step is followed by the step of inspecting the polished implant to determine the extent of polishing and thereafter repeating the contacting, moving, and washing steps if more polishing is needed.
Claim 7
Dependent Claim
72 words
A polished surgical ear tube implant comprising an ear tube surgical implant formed of a biocompatible titanium or titanium alloy polished to a smooth, matte finish by contacting the formed implant with a polishing solution including lactic acid, hydrofluoric acid, and nitric acid; a. moving the implant and solution relative to one another; and thereafter b. washing the implant to remove substantially all of the polishing solution to produce the polished implant.
Claim 8
Dependent Claim
72 words
A polished surgical ear tube implant comprising an ear tube surgical implant formed of a biocompatible titanium or titanium alloy polished to a smooth, matte finish by contacting the formed implant with a polishing solution including lactic acid, hydrofluoric acid, and nitric acid; a. moving the implant and solution relative to one another; and thereafter b. washing the implant to remove substantially all of the polishing solution to produce the polished implant.
Claim 9
Dependent Claim
44 words
The polished ear tube implant of claim 6 wherein the polishing solution comprises: from about 60 to about 79 weight percent lactic acid; from about 10.5 to about 20 weight percent hydroflouric acid; and from about 10.5 to about 20 weight percent nitric acid.
Claim 10
Dependent Claim
22 words
The polished ear tube implant of claim 7 wherein the immersed implant is polished by agitating the immersed implant in the solution.
Claim 11
Dependent Claim
46 words
The polished ear tube implant of claim 8 wherein the formed implant is an ear tube having machining grooves therein and wherein the contacting, moving, and washing steps are repeated to substantially decrease the depth of the grooves to produce a smooth, matte finished ear tube.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-11-02 | 1991-05-04 | 1991-11-03 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-11-02 | 1995-05-04 | 1995-11-03 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-11-02 | 1999-05-04 | 1999-11-03 | $7700.00 | Window Closed / Lapsed |