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Method of manufacture of multifilamentary intermetallic superconductors

Assignee: Airco Inc
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Filing: 1982-09-29
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Granted: 1983-10-25
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Expires: 2002-09-29
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Abstract

Abstract An improved method for manufacture of multifilamentary superconductors of the A 3 B type having the A-15 crystal structure, such as Nb 3 Sn, is disclosed in which rods or wires of the A material are disposed throughout a matrix consisting of Cu and the B material in substantially elemental form. The matrix is formed by compaction of powders of Cu; powders of the B may be mixed therewith or the B material may be infiltrated into pores between the individual Cu particles after compaction. The resultant composite has A, B and Cu distributed uniformly throughout its volume and can be worked to any desired final shape and size for heat treatment to form the A 3 B material without intermediate annealing steps.

Inventors

  • 👤 William G. Marancik

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 17:52
CPC Classifications
H; H10; H10N; H10N60/00; H10N60/01; H10N60/0184; Y; Y10; Y10S; Y10S505/00; Y10S505/80; Y10S505/815; Y10S505/823; Y10S505/825; Y10S505/917; Y10S505/918; Y10S505/919; Y10S505/921; Y10T; Y10T29/00; Y10T29/49; Y10T29/49002; Y10T29/49014

Claims Analysis

Total Claims: 19
Claim 1
Independent Claim 170 words
A method for manufacturing a multifilamentary superconductor having the composition A 3 B and the A-15 crystal structure, comprising the following steps: encasing one or more rods or wires of the A material within a sheath of a material consisting essentially of a compacted composite of Cu and the B material said composite being formed by compaction of Cu powder into a porous matrix, sintering said porous matrix, and dipping said porous matrix into a bath of the B material, whereby said B material is infiltrated into the pores in said sintered porous Cu matrix; working the sheathed rods to firmly consolidate said composite upon said rods; packing a plurality of the worked sheathed rods together; further working the assembled plurality of sheathed rods to a desired final shape and size; and subjecting the worked assembly to a heat treatment for a time and at a temperature such that the compound A 3 B is formed at the interfaces between the rods of the A material and the composite material.
Claim 2
Independent Claim 170 words
A method for manufacturing a multifilamentary superconductor having the composition A 3 B and the A-15 crystal structure, comprising the following steps: encasing one or more rods or wires of the A material within a sheath of a material consisting essentially of a compacted composite of Cu and the B material said composite being formed by compaction of Cu powder into a porous matrix, sintering said porous matrix, and dipping said porous matrix into a bath of the B material, whereby said B material is infiltrated into the pores in said sintered porous Cu matrix; working the sheathed rods to firmly consolidate said composite upon said rods; packing a plurality of the worked sheathed rods together; further working the assembled plurality of sheathed rods to a desired final shape and size; and subjecting the worked assembly to a heat treatment for a time and at a temperature such that the compound A 3 B is formed at the interfaces between the rods of the A material and the composite material.
Claim 3
Dependent Claim 17 words
The method of claim 1 wherein the A material is Nb and the B material is Sn.
Claim 4
Dependent Claim 17 words
The method of claim 1 wherein the A material is V and the B material is Ga.
Claim 5
Independent Claim 138 words
A method of manufacture of a multifilamentary superconductor of the type in which a predetermined number of fine filaments of intermetallic superconductive material having the composition A 3 B and the A-15 crystal structure are embedded in a matrix of normal conductor, which comprises: disposing wires of the A material in a matrix consisting of Cu and the B material, said Cu and said B material having substantially unalloyed, said matrix being formed by compaction of elemental powder of Cu to form a porous matrix and susequent infiltration of the B material into the pores of said porous matrix; working the assembly of wires of the A material and said matrix to a desired final shape and size; and performing a heat treatment to form said superconductive compound at the interfaces between said wires and said composite matrix.
Claim 6
Independent Claim 138 words
A method of manufacture of a multifilamentary superconductor of the type in which a predetermined number of fine filaments of intermetallic superconductive material having the composition A 3 B and the A-15 crystal structure are embedded in a matrix of normal conductor, which comprises: disposing wires of the A material in a matrix consisting of Cu and the B material, said Cu and said B material having substantially unalloyed, said matrix being formed by compaction of elemental powder of Cu to form a porous matrix and susequent infiltration of the B material into the pores of said porous matrix; working the assembly of wires of the A material and said matrix to a desired final shape and size; and performing a heat treatment to form said superconductive compound at the interfaces between said wires and said composite matrix.
Claim 7
Dependent Claim 17 words
The method of claim 4 wherein the A material is Nb and the B material is Sn.
Claim 8
Dependent Claim 18 words
The method according to claim 4 wherein the A material is V and the B material is Ga.
Claim 9
Independent Claim 90 words
The method for manufacture of multifilamentary superconductive wire, comprising the steps of: preparing a composite material, consisting essentially of Cu and Sn, by compaction of powders; sheathing rods of Nb in strips of said composite material; drawing said sheathed Nb rods to an intermediate size; packing a plurality of said drawn rods within a generally tubular structure; reducing said tubular structure containing said rods to a desired final shape and size; and heat treating said structure at its final size to form Nb 3 Sn about said rods of Nb.
Claim 10
Independent Claim 90 words
The method for manufacture of multifilamentary superconductive wire, comprising the steps of: preparing a composite material, consisting essentially of Cu and Sn, by compaction of powders; sheathing rods of Nb in strips of said composite material; drawing said sheathed Nb rods to an intermediate size; packing a plurality of said drawn rods within a generally tubular structure; reducing said tubular structure containing said rods to a desired final shape and size; and heat treating said structure at its final size to form Nb 3 Sn about said rods of Nb.
Claim 11
Dependent Claim 33 words
The method of claim 7 wherein said composite is formed by compaction of Cu powders into a porous matrix, sintering of said matrix, and subsequent infiltration of Sn into pores of said matrix.
Claim 12
Dependent Claim 35 words
The method of claim 8 further comprising the additional step of heat treatment of said infiltrated matrix prior to said sheathing step at a temperature such that said Sn does not alloy with said Cu.
Claim 13
Dependent Claim 20 words
The method of claim 7 wherein said composite is formed by compaction of a mixture of Cu and Sn powders.
Claim 14
Dependent Claim 30 words
The method of claim 10 further comprising the additional step of heat treatment of said Cu/Sn composite at a temperature such that said Sn and said Cu do not alloy.
Claim 15
Dependent Claim 38 words
The method of claim 7 wherein an intermediate heat treatment is performed on said structure containing said rods prior to the heat treatment during which Nb 3 Sn is formed, during which said Sn and Cu are alloyed.
Claim 16
Dependent Claim 30 words
The method of claim 12 wherein mechanical working is performed on said structure containing said rods after said intermediate heat treatment, to eliminate porosity formed during said intermediate heat treatment.
Claim 17
Dependent Claim 136 words
In a method of manufacture of a multifilamentary superconductor of the A-15 type having the composition A 3 B, comprising the steps of forming a precursor assembly comprising Cu, A and B, said A being disposed in filamentary form substantially uniformly throughout a matrix of Cu and B, said matrix being formed by compaction of Cu powder into a porous matrix, sintering said porous matrix and subsequent infiltration of the B material into the pores of said porous matrix, working said assembly to a desired finished shape and size, and performing a reaction heat treatment to form A 3 B at the interfaces between said A filaments and the matrix, the improvement which comprises said Cu and B materials being substantially not alloyed during said working, and said B material being disposed uniformly throughout said matrix.
Claim 18
Dependent Claim 136 words
In a method of manufacture of a multifilamentary superconductor of the A-15 type having the composition A 3 B, comprising the steps of forming a precursor assembly comprising Cu, A and B, said A being disposed in filamentary form substantially uniformly throughout a matrix of Cu and B, said matrix being formed by compaction of Cu powder into a porous matrix, sintering said porous matrix and subsequent infiltration of the B material into the pores of said porous matrix, working said assembly to a desired finished shape and size, and performing a reaction heat treatment to form A 3 B at the interfaces between said A filaments and the matrix, the improvement which comprises said Cu and B materials being substantially not alloyed during said working, and said B material being disposed uniformly throughout said matrix.
Claim 19
Dependent Claim 32 words
The method of claim 14 wherein said assembly is formed by packing together a plurality of rods of the A material, each sheathed in a composite of Cu and the B material.

References Cited (Backward Citations)

US3277557A Cited
US3496622A Cited
US3541680A Cited
US3472705A Cited
US3509622A Cited
US4044457A Cited
US4223434A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-10-24 1987-04-25 1987-10-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-10-24 1991-04-25 1991-10-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-10-24 1995-04-25 1995-10-25 $7700.00 Window Closed / Lapsed

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