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US4281029A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of coating with a stoichiometric compound

Assignee: Futaba Corp
•
Filing: 1979-10-01
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Granted: 1981-07-28
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Expires: 1999-10-01
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Abstract

Abstract A method of coating which comprises the steps of separately vaporizing a plurality of substances containing the component elements of a desired compound and placed in a plurality of crucibles to form vapors of the substances, mixing the vapors in a heated mixing chamber to form a mixed vapor, jetting the mixed vapor into a vacuum region to form clusters, ionizing the clusters to form cluster ions, and accelerating the cluster ions to make them impinge on a substrate. An apparatus for coating which comprises a plurality of crucibles for separately vaporizing substances containing the component elements of a desired compound to form vapors of the substances, a mixing chamber for heating and mixing the vapors introduced therein to form a mixed vapor, the mixing chamber having at least one injection hole for jetting the mixed vapor into a vacuum region, communication pipes for connecting the mixing chamber to the crucibles, an ionization chamber for ionizing clusters produced from the mixed vapor jetted from the mixing chamber, means for accelerating cluster ions produced in the ionization chamber and making them impinge on a substrate, and a substrate holder for holding the substrate.

Inventors

  • 👤 Toshinori Takagi
  • 👤 Kiyoshi Morimoto
  • 👤 Hiroshi Watanabe

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-22 20:11
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; C23C14/228; C23C14/221; C23C14/24; C23C14/243; C30; C30B; C30B23/00; C30B23/02; C30B23/08; Y; Y10; Y10S; Y10S148/00; Y10S148/006; Y10S148/045; Y10S148/064; Y10S148/065; Y10S148/072; Y10S148/169; Y10S438/00; Y10S438/935; Y10S438/961; Y10S438/971

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 139 words
A method of producing compounds which comprises the steps of separately heating and vaporizing a plurality of substances-to-be-vaporized containing the component elements of a desired compound and placed in a plurality of crucibles respectively to form vapors of said substances, the degree of heating of said crucible being proportional to the vapor pressure of the substance contained therein, feeding said vapors into a heated mixing chamber in a stoichiometric proportion and mixing said vapors therein to form a mixed vapor, jetting said mixed vapor through an aperture in said mixing chamber and into a vacuum region to form clusters, and making said clusters impinge on a substrate under the influence of injection energy given to said clusters when jetted, wherein during the feeding of said vapors into said mixing chamber, said vapors are not initially directed towards said aperture.
Claim 2
Independent Claim 139 words
A method of producing compounds which comprises the steps of separately heating and vaporizing a plurality of substances-to-be-vaporized containing the component elements of a desired compound and placed in a plurality of crucibles respectively to form vapors of said substances, the degree of heating of said crucible being proportional to the vapor pressure of the substance contained therein, feeding said vapors into a heated mixing chamber in a stoichiometric proportion and mixing said vapors therein to form a mixed vapor, jetting said mixed vapor through an aperture in said mixing chamber and into a vacuum region to form clusters, and making said clusters impinge on a substrate under the influence of injection energy given to said clusters when jetted, wherein during the feeding of said vapors into said mixing chamber, said vapors are not initially directed towards said aperture.
Claim 3
Dependent Claim 44 words
The method of producing compounds as set forth in claim 1, wherein said step of mixing the vapors of said substances-to-be-vaporized further comprises mixing the vapors of said substances with vapors or gases of impurities for determining the conduction type of the desired compound.
Claim 4
Independent Claim 143 words
A method of producing compounds which comprises the steps of separately heating and vaporizing a plurality of substances-to-be-vaporized containing the component elements of a desired compound and placed in a plurality of crucibles respectively to form vapors of said substances the degree of heating of each said crucible proportional to the vapor pressure of the substance contained therein, feeding said vapors into a heated mixing chamber in a stoichiometric proportion and mixing said vapors therein to form a mixed vapor, jetting said mixed vapor through an aperture in said mixing chamber and into a vacuum region to form clusters, ionizing said clusters to form cluster ions, and giving kinetic energy to said cluster ions thereby making said cluster ions impinge on a substrate, wherein during the feeding of said vapors into said mixing chamber, said vapors are not initially directed towards said aperture.
Claim 5
Independent Claim 143 words
A method of producing compounds which comprises the steps of separately heating and vaporizing a plurality of substances-to-be-vaporized containing the component elements of a desired compound and placed in a plurality of crucibles respectively to form vapors of said substances the degree of heating of each said crucible proportional to the vapor pressure of the substance contained therein, feeding said vapors into a heated mixing chamber in a stoichiometric proportion and mixing said vapors therein to form a mixed vapor, jetting said mixed vapor through an aperture in said mixing chamber and into a vacuum region to form clusters, ionizing said clusters to form cluster ions, and giving kinetic energy to said cluster ions thereby making said cluster ions impinge on a substrate, wherein during the feeding of said vapors into said mixing chamber, said vapors are not initially directed towards said aperture.
Claim 6
Dependent Claim 44 words
The method of producing compounds as set forth in claim 3, wherein said step of mixing the vapors of said substances-to-be-vaporized further comprises mixing the vapors of said substances with vapors or gases of impurities for determining the conduction type of the desired compound.

References Cited (Backward Citations)

US3127226A Cited
US3839084A Cited
US3974059A Cited
DE2547552A1 Cited
US4082636A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-07-27 1985-01-26 1985-07-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-07-27 1989-01-26 1989-07-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-07-27 1993-01-26 1993-07-28 $7700.00 Window Closed / Lapsed

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