← Back to Patent Explorer
US4254159A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of producing gold-color coatings

Assignee: OC Oerlikon Balzers AG
•
Filing: 1978-12-20
•
Granted: 1981-03-03
•
Expires: 1998-12-20
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A method of producing gold-color coatings on substrates by evaporating a coating material comprising a metallic titanium or zirconium in a housing which has walls which define an evaporation space, comprises, maintaining a vacuum atmosphere containing N 2 and argon in the space. The method is carried out using an anode connected to a power source to produce a low voltage arc discharge in the vicinity of the coating material which is arranged within the evaporation space and also maintaining a low voltage arc between the anode and the substrates. A potential difference between the anode and the substrates of a range of between 5 v and 100 v are maintained during the process and, in addition, the electrical potential of the substrates is maintained between 0 and 150 volts lower than the potential of the housing walls which define the evaporation space. The substrate to be coated is coated at a rate of from between 1 to 15 nanometers per second. The N 2 and argon atmosphere is maintained so that a partial pressure of the N 2 -containing component ranges between 2×10 -4 and 10 -2 millbar. The potential difference between the anode and the substrates is reduced in the course of the process to release the sputtering threshold of the substrate and the housing wall. The partial pressure of the N 2 -containing components continuously increase in the course of the process.

Inventors

  • 👤 Hans K. Pulker
  • 👤 Helmut Daxinger

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 13:10
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/0021; C23C14/22; C23C14/24; C23C14/32; G; G04; G04B; G04B37/00; G04B37/22

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 163 words
A method of producing gold-color coatings on substrates by evaporating a coating material of metallic titanium or zirconium in a housing having walls defining an evaporation space with a vacuum atmosphere containing N 2 and argon and using an anode connected to a power source to produce a low voltage arc discharge in the vicinity of the coating material and between the anode and a cathode, comprising, maintaining a potential difference between the anode and the substrates with the anode positive with respect to the substrates of a range of from between 5 and 100 volts, maintaining the electrical potential of the substrates between from 0 to 150 volts lower than the potential of the housing walls defining the evaporation space, coating the substrate at a rate of from between 1 and 15 nanometers per second, and maintaining the N 2 and argon atmosphere so that the partial pressure of the N 2 -containing component ranges between 2×10 -4 and 10 -2 millibars.
Claim 2
Independent Claim 163 words
A method of producing gold-color coatings on substrates by evaporating a coating material of metallic titanium or zirconium in a housing having walls defining an evaporation space with a vacuum atmosphere containing N 2 and argon and using an anode connected to a power source to produce a low voltage arc discharge in the vicinity of the coating material and between the anode and a cathode, comprising, maintaining a potential difference between the anode and the substrates with the anode positive with respect to the substrates of a range of from between 5 and 100 volts, maintaining the electrical potential of the substrates between from 0 to 150 volts lower than the potential of the housing walls defining the evaporation space, coating the substrate at a rate of from between 1 and 15 nanometers per second, and maintaining the N 2 and argon atmosphere so that the partial pressure of the N 2 -containing component ranges between 2×10 -4 and 10 -2 millibars.
Claim 3
Dependent Claim 46 words
A method of producing gold-color coatings, as claimed in claim 1, wherein the potential difference between the anode and the substrates is reduced in the course of the process to at least the sputtering threshold of the substrate and/or the housing walls defining the evaporation space.
Claim 4
Dependent Claim 30 words
A method of producing gold-color coatings, as claimed in claim 1, wherein the partial pressure of the N 2 -containing component is continuously increased in the course of the process.

References Cited (Backward Citations)

US3953619A Cited
DE2410483A1 Cited
US3900592A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-03-02 1984-09-01 1985-03-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-03-02 1988-09-01 1989-03-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-03-02 1992-09-01 1993-03-03 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag