Patent US4188236A successfully refreshed from Google Patents.
US4188236A
Expired / Lapsed
US
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Process for the production of a pigment composition
Assignee: BASF Corp
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Filing: 1978-11-09
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Granted: 1980-02-12
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Expires: 1998-11-09
Abstract
Abstract A process for the production of a non-dusting pigment composition by contacting an aqueous dispersion of an organic pigment with (a) a solution or dispersion of an alkaline soluble rosin acid derivative (b) a sorbitan ester, and (c) a water-insoluble organic carrier having a melting point below 100 DEG C. at a temperature above the melting point of both the sorbitan ester and the organic carrier, reducing the pH to below epsilon , stirring the composition until the pigment, rosin derivative, sorbitan ester and organic carrier are associated in generally spherical granules and recovering the resulting granules.
Inventors
- 👤 George H. Robertson
- 👤 Alistair B. Boyd
- 👤 Robert L. Rooney
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 17:19
CPC Classifications
C; C09; C09B; C09B67/00; C09B67/0071; C09B67/0092; C09B67/006
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
143 words
A process for the production of a pigment composition in a non-dusting form which comprises contacting an aqueous dispersion of an organic pigment with (a) a solution or dispersion of an alkaline soluble rosin acid derivative having an approximate acid value in the range 100-250 at a pH of from 8 to 11 (b) a sorbitan ester, and (c) a water-insoluble organic carrier having a melting point below 100° C. at a temperature above the melting point of both the sorbitan ester and the organic carrier, reducing th pH to below 8, stirring the composition until the pigment, rosin derivative, sorbitan ester and organic carrier are associated in generally spherical granules, and recovering the resulting granules, the amounts of ingredients being 40-75% pigment, 5-25% rosin acid, 5-40% sorbitan ester and 5-50% carrier, all percentages being based on the weight of the total composition.
Claim 2
Dependent Claim
143 words
A process for the production of a pigment composition in a non-dusting form which comprises contacting an aqueous dispersion of an organic pigment with (a) a solution or dispersion of an alkaline soluble rosin acid derivative having an approximate acid value in the range 100-250 at a pH of from 8 to 11 (b) a sorbitan ester, and (c) a water-insoluble organic carrier having a melting point below 100° C. at a temperature above the melting point of both the sorbitan ester and the organic carrier, reducing th pH to below 8, stirring the composition until the pigment, rosin derivative, sorbitan ester and organic carrier are associated in generally spherical granules, and recovering the resulting granules, the amounts of ingredients being 40-75% pigment, 5-25% rosin acid, 5-40% sorbitan ester and 5-50% carrier, all percentages being based on the weight of the total composition.
Claim 3
Dependent Claim
25 words
A process as claimed in claim 1, in which the rosin acid derivative is based on wood rosin or its hydrogenated derivative or disproportionated rosin.
Claim 4
Dependent Claim
24 words
A process as claimed in claim 1, in which the sorbitan ester is derived from a fatty acid having 12 to 22 carbon atoms.
Claim 5
Dependent Claim
30 words
A process as claimed in claim 1, in which the organic carrier is a single compound or a mixture of compounds which give a mixed melting point below 100° C.
Claim 6
Dependent Claim
17 words
A process as claimed in claim 1, in which a protective colloid is added to the mixture.
Claim 7
Dependent Claim
22 words
A process as claimed in claim 1, in which the amount of pigment is from 50-60% by weight of the total composition.
Claim 8
Dependent Claim
25 words
A process as claimed in claim 1, in which the amount of sorbitan ester is from 10 to 20% by weight of the total composition.
Claim 9
Dependent Claim
25 words
A process as claimed in claim 1, in which the amount of organic carrier is from 20 to 30% by weight of the total composition.
Claim 10
Dependent Claim
26 words
A process as claimed in claim 1, in which up to 2% by weight of a finely divided silica or silicate is added to the mixture.
References Cited (Backward Citations)
US4015999A
Cited
US4116924A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1983-02-11 | 1983-08-13 | 1984-02-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1987-02-11 | 1987-08-13 | 1988-02-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1991-02-11 | 1991-08-13 | 1992-02-12 | $7700.00 | Window Closed / Lapsed |