Patent US4125446A successfully refreshed from Google Patents.
US4125446A
Expired / Lapsed
US
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Controlled reflectance of sputtered aluminum layers
Assignee: Airco Inc
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Filing: 1977-08-15
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Granted: 1978-11-14
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Expires: 1997-08-15
Abstract
Abstract A method for depositing aluminum layers having a predetermined reflectance or a predetermined resistivity is disclosed. The layers are deposited by sputtering a target comprising 90% or greater aluminum. The parameters which must be controlled include the partial pressure of reactive gases, such as nitrogen, hydrogen, oxygen and water vapor, which are minor constituents of the sputtering gas, the total sputtering gas pressure, the substrate temperature, and the deposition rate.
Inventors
- 👤 Larry D. Hartsough
- 👤 Paul S. McLeod
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 06:16
CPC Classifications
C; C03; C03C; C03C17/00; C03C17/06; C03C17/09; C23; C23C; C23C14/00; C23C14/0021; C23C14/0036; C23C14/0042; F; F21; F21V; F21V7/00; F21V7/22; F21V7/24; F21V7/28; F24; F24S; F24S23/00; F24S23/70; F24S23/82; Y; Y02; Y02E; Y02E10/00; Y02E10/40
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
99 words
A method for depositing an aluminum layer having a predetermined reflectance comprising: placing a target comprising at least 90% aluminum and a substrate in a evacuable chamber; evacuating the chamber; introducing a reactive gas into the chamber at a controlled rate to provide a predetermined partial pressure of 10 -7 to 10 -4 torr; providing an ionizable inert gas in the chamber to maintain the total pressure of 5 × 10 -4 to 5 × 10 -2 torr; and applying an electric potential to the target to sputter the target and deposit a layer of material on the substrate.
Claim 2
Independent Claim
99 words
A method for depositing an aluminum layer having a predetermined reflectance comprising: placing a target comprising at least 90% aluminum and a substrate in a evacuable chamber; evacuating the chamber; introducing a reactive gas into the chamber at a controlled rate to provide a predetermined partial pressure of 10 -7 to 10 -4 torr; providing an ionizable inert gas in the chamber to maintain the total pressure of 5 × 10 -4 to 5 × 10 -2 torr; and applying an electric potential to the target to sputter the target and deposit a layer of material on the substrate.
Claim 3
Dependent Claim
23 words
The method according to claim 1 wherein the reactive gas is selected from the group consisting of nitrogen, hydrogen, oxygen and water vapor.
Claim 4
Dependent Claim
16 words
The method according to claim 2 wherein the deposited layer is greater than 0.5 μm thick.
Claim 5
Dependent Claim
18 words
The method according to claim 3 wherein the layer is deposited at a rate greater than 10 nm/sec.
Claim 6
Dependent Claim
20 words
The method according to claim 4 further comprising heating the substrates to an initial temperature of 30° to 250° C.
Claim 7
Dependent Claim
21 words
The method according to claim 5 further comprising magnetically confining a glow discharge plasma to a closed loop adjacent the target.
Claim 8
Dependent Claim
16 words
The method according to claim 6 wherein the source-to substrate distance is 3 to 9 cm.
Claim 9
Dependent Claim
19 words
The method according to claim 7 wherein the total pressure is 10 -3 to 2.5 × 10 -2 torr.
Claim 10
Dependent Claim
34 words
The method according to claim 8 wherein the target material is selected from the group consisting essentially of 99% or greater Al, Al -- 2% Si and Al -- 4% Cu -- 2% Si.
Claim 11
Dependent Claim
32 words
The method according to claim 9 wherein the reactive gas is nitrogen at a pressure of 10 -7 to 10 -5 torr, and the initial substrate temperature is less than 85° C.
Claim 12
Dependent Claim
13 words
The method according to claim 9 wherein the reactive gas is water vapor.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-11-13 | 1982-05-15 | 1982-11-14 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-11-13 | 1986-05-15 | 1986-11-14 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-11-13 | 1990-05-15 | 1990-11-14 | $7700.00 | Window Closed / Lapsed |