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US3906116A Expired / Lapsed US ⏱️ 0.0 years remaining

Concentrated oleoresin products and emulsification process for preparing them

Assignee: Bush Boake Allen Ltd
•
Filing: 1973-09-24
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Granted: 1975-09-16
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Expires: 1993-09-24
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Abstract

Abstract Concentrated emulsions of flavor oleoresins are prepared by (1) forming a solution or colloidal solution of the oleoresin in a diluent; (2) forming a preformed mixture comprising an emulsion stabilizer and at least one oil selected from the group consisting of edible and essential oils; (3) mixing said solution or colloidal solution with said preformed mixture with agitation; (4) adding an aqueous solution or dispersion of an emulsion stabilizer to form a final mixture; and (5) emulsifying said final mixture. The product aqueous emulsion may be spray dried to form an encapsulated oleoresin.

Inventors

  • 👤 Peter Gregory Quesnel
  • 👤 Andreas Lambrou
  • 👤 Edwin Stanley Walker

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 07:35
CPC Classifications
A; A23; A23L; A23L27/00; A23L27/80

Claims Analysis

Total Claims: 23
Claim 1
Independent Claim 94 words
A PROCESS FOR PREPARING AN AQUEOUS EMULSION OF A FLAVOUR OLEORESIN WHICH PROCESS COMPRISES FORMING, AN OLEORESIN SOLUTION OR COLLODIAL SOLUTION (A) OF THE OLEORESIN IN A DILUENT, MIXING SAID SOLUTION OR COLLODIAL SOLUTION (A) WITH AGITATION WITH A PREFORMED MIXTURE (B) COMPRISING AN EMULSION STABILISER, AND AT LEAST ONE OIL SELECTED FROM THE GROUP CONSISTING OF EDIBLE OILS AND ESSENTIAL OILS, ADDING AN AQUEOUS SOLUTION OR DISPERSION (C) OF AN EMULSION STABILISER TO FORM A FINAL MIXTURE (D), AND EMULSIFYING SAID FINAL MIXTURE (D) TO FORM AN AQUEOUS EMULSION OF SAID FLAVO OLEORESIN.
Claim 2
Dependent Claim 94 words
A PROCESS FOR PREPARING AN AQUEOUS EMULSION OF A FLAVOUR OLEORESIN WHICH PROCESS COMPRISES FORMING, AN OLEORESIN SOLUTION OR COLLODIAL SOLUTION (A) OF THE OLEORESIN IN A DILUENT, MIXING SAID SOLUTION OR COLLODIAL SOLUTION (A) WITH AGITATION WITH A PREFORMED MIXTURE (B) COMPRISING AN EMULSION STABILISER, AND AT LEAST ONE OIL SELECTED FROM THE GROUP CONSISTING OF EDIBLE OILS AND ESSENTIAL OILS, ADDING AN AQUEOUS SOLUTION OR DISPERSION (C) OF AN EMULSION STABILISER TO FORM A FINAL MIXTURE (D), AND EMULSIFYING SAID FINAL MIXTURE (D) TO FORM AN AQUEOUS EMULSION OF SAID FLAVO OLEORESIN.
Claim 3
Dependent Claim 26 words
A process according to claim 1 wherein the oleoresin is at least one oleoresin selected from the group consisting of pepper, turmeric, cinnamon and mushroom oleoresins.
Claim 4
Dependent Claim 32 words
A process according to claim 2 wherein there is obtained an emulsion containing at least 20% by weight of pepper oleoresin (based on the weight of the non-aqueous components of the emulsion).
Claim 5
Dependent Claim 15 words
A process according to claim 1 wherein the diluent is ethanol, isopropanol, or propylene glycol.
Claim 6
Dependent Claim 24 words
A process according to claim 1 wherein the weight of diluent in said solution (a) is 25 - 120% of the weight of oleoresin.
Claim 7
Dependent Claim 30 words
A process according to claim 1 wherein 2 - 4 parts by weight of solution or colloidal solution (a) are mixed with 1 part by weight of the mixture (b).
Claim 8
Dependent Claim 24 words
A process according to claim 1 wherein the preformed mixture (b) contains emulsion stabilizer and oil in a weight ratio of 1.5:1 to 3:1
Claim 9
Dependent Claim 32 words
A process according to claim 1 wherein the weight of stabiliser in the aqueous solution or dispersion (c) is two to six times the weight of stabilizer in the preformed mixture (b).
Claim 10
Dependent Claim 23 words
A process according to claim 1 wherein an emulsifying agent is added during said mixing of solution (a) with the preformed mixture (b).
Claim 11
Dependent Claim 24 words
A process according to claim 1 wherein the stabilizer is at least one stabilizer selected from the group consisting of gum acacia and maltodextrin.
Claim 12
Dependent Claim 17 words
A process according to claim 1 wherein the edible oil is arachis oil or cotton seed oil.
Claim 13
Dependent Claim 36 words
A process according to claim 3 wherein said emulsion stabilizer is at least one stabilizer selected from the group consisting of gum acacia and maltodextrin, and wherein said oil is arachis oil or cotton seed oil.
Claim 14
Dependent Claim 26 words
A process according to claim 1 wherein there is obtained an emulsion containing at least 8% of oleoresin based on the weight of the non-aqueous components.
Claim 15
Dependent Claim 26 words
A process according to claim 2 wherein there is obtained an emulsion containing at least 8% of oleoresin based on the weight of the non-aqueous components.
Claim 16
Dependent Claim 87 words
A process according to claim 14 wherein the weight of diluent is 25-120% of the weight of oleoresin; wherein the preformed mixture (b) contains emulsion stabilizer and oil in a weight ratio of 1.5:1 to 3:1, wherein 2-4 parts by weight of solution or colloidal solution (a) are mixed with 1 part by weight of the preformed mixture (b); and wherein the weight of stabilizer in the aqueous solution or dispersion (c) is two to six times the weight of the stabilizer in the preformed mixture (b).
Claim 17
Dependent Claim 11 words
A process according to claim 15 wherein the diluent is ethanol.
Claim 18
Dependent Claim 12 words
A process according to claim 15 wherein the diluent is Propylene glycol.
Claim 19
Dependent Claim 23 words
A process according to claim 15 wherein an emulsifying agent is added during said mixing of solution (a) with the preformed mixture (b).
Claim 20
Dependent Claim 24 words
A process according to claim 15 wherein the stabilizer is at least one stabilizer selected from the group consisting of gum acacia and maltodextrin.
Claim 21
Dependent Claim 18 words
A process according to claim 15 wherein said preformed mixture (b) comprises an emulsion stabilizer and arachis oil.
Claim 22
Dependent Claim 19 words
A process according to claim 15 wherein said preformed mixture (b) comprises an emulsion stabilizer and cotton seed oil.
Claim 23
Dependent Claim 160 words
A process according to claim 3 wherein said emulsion contains between 20 and 35% pepper oleoresin; wherein said diluent is ethanol or propylene glycol; wherein the weight of said diluent in said solution is 25-120% of the weight of the oleoresin; wherein the preformed mixture (b) contains emulsion stabilizer and oil in a weight ratio of 1.5:1 to 3:1; wherein the weight of stabilizer in the aqueous solution or dispersion (c) is two to six times the weight of stabilizer in the preformed mixture (b); wherein 2-4 parts by weight of solution or colloidal solution (a) are mixed with 1 part by weight of the mixture (d); wherein an emulsifying agent is added during said mixing of solution (a) with the preformed mixture (d); wherein the stabilizer is at least one stabilizer selected from the group consisting of gum acacia and maltodextrin; and wherein the said preformed mixture (b) comprises an emulsion stabilizer and arachis oil or cotton seed oil.

References Cited (Backward Citations)

US1545993A Cited
US3091567A Cited
US3582361A Cited
US3819838A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-09-15 1979-03-17 1979-09-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-09-15 1983-03-17 1983-09-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-09-15 1987-03-17 1987-09-16 $7700.00 Window Closed / Lapsed

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