US5133756A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for producing a bone replacement material
Assignee: Biomet Deutschland GmbH
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Filing: 1988-08-09
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Granted: 1992-07-28
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Expires: 2008-08-09
Abstract
Abstract According to a process for producing a bone replacement material, natural bones are used as raw material, the soft parts of the bones are removed, as well as any residual organic substances, and the remaining osseous substance is finally sintered at temperatures between 1100 degrees and 1500 degrees Celcius. In order to simplify such a process and to ensure a more gentle processing of the inorganic bone matrix, the bones are dried at an increased temperature, maximum 550 degrees Celcius, with a reduced air supply or in a reducing atmosphere, then the temperature of the bones is increased during the following step up to 750 degrees to 800 degrees Celcius, with an increased air supply, and finally the bones are sintered.
Inventors
- 👤 Gerd Bauer
- 👤 Freimut Vizethum
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 15:28
CPC Classifications
A; A61; A61L; A61L27/00; A61L27/36; A61L27/3604; A61L27/3608; A61L27/3641; A61L27/3645; A61L27/365; A61L27/3683; A61L27/3691; Y; Y10; Y10S; Y10S623/00; Y10S623/901; Y10S623/915; Y10S623/919
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
123 words
In a process for producing a bone replacement material in which natural bones are used as starting material, soft tissues are removed from the bone, a removal of residual substances is effected and remaining osseous substance is then sintered at temperatures between 1100° and 1500° C., the improvement wherein: the bone is dried at an elevated temperature of up to a maximum of 150° C. after removal of the soft tissues; the temperature is then raised to about 550° C. wherein pyrolysis occurs with a reduced air supply or in a reducing atmosphere; and in a following step the bone is heated to a temperature of between 750° and 800° C. with an increased air supply, and in that sintering takes place subsequently.
Claim 2
Dependent Claim
123 words
In a process for producing a bone replacement material in which natural bones are used as starting material, soft tissues are removed from the bone, a removal of residual substances is effected and remaining osseous substance is then sintered at temperatures between 1100° and 1500° C., the improvement wherein: the bone is dried at an elevated temperature of up to a maximum of 150° C. after removal of the soft tissues; the temperature is then raised to about 550° C. wherein pyrolysis occurs with a reduced air supply or in a reducing atmosphere; and in a following step the bone is heated to a temperature of between 750° and 800° C. with an increased air supply, and in that sintering takes place subsequently.
Claim 3
Dependent Claim
29 words
A process according to claim 1, wherein the bone is dried at an elevated temperature of up to a maximum of 150° C. for between 24 and 72 hours.
Claim 4
Dependent Claim
24 words
A process according to claim 1 wherein, during drying, the temperature is gradually increased from ambient temperature to the maximum temperature of 150° C.
Claim 5
Dependent Claim
30 words
A process according to claim 1, wherein the bone is treated for approximately 8 to 24 hours during the step with a reduced air supply or in a reducing atmosphere.
Claim 6
Dependent Claim
31 words
A process according to claim 1 wherein the temperature is gradually increased to 550° C. during the treatment of the bone with a reduced air supply or in a reducing atmosphere.
Claim 7
Dependent Claim
34 words
A process according to claim 1, wherein the bone is kept at a maximum temperature of 760° to 800° C. for approximately 4 to 24 hours during the step with an increased air supply.
Claim 8
Dependent Claim
25 words
A process according to claim 1 wherein the temperature is gradually increased to approximately 800° C. when incinerating the bone with an increased air supply.
Claim 9
Dependent Claim
25 words
A process according to claim 1, wherein the sintering is carried out for 2 to 20 hours at maximum temperatures of 1100° to 1400° C.
Claim 10
Dependent Claim
20 words
A process according to claim 1, wherein the temperature during sintering is gradually increased to the maximum temperature of sintering.
Claim 11
Dependent Claim
32 words
A process according to claim 1, wherein, after sintering, the bone is, during cooling, kept at a temperature of between 1120° to 1160° C. for a period of 2 to 6 hours.
References Cited (Backward Citations)
US4314380A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-07-28 | 1996-01-27 | 1996-07-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-07-28 | 2000-01-27 | 2000-07-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-07-28 | 2004-01-27 | 2004-07-28 | $7700.00 | Window Closed / Lapsed |