US4423303A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Apparatus for treating powdery materials utilizing microwave plasma
Assignee: Toshiba Corp
•
Filing: 1981-05-05
•
Granted: 1983-12-27
•
Expires: 2001-05-05
Abstract
Abstract The apparatus includes a microwave generating device and, a waveguide connected with the microwave generating device. A reaction vessel disposed through the waveguide and supplied with a powdery material to be treated with a reaction gas. Pumps are provided for exhausting the reaction vessel. The reaction vessel comprises a vertically elongated vessel having a bottom above which a plasma generating area is formed. In one embodiment, the reaction vessel further comprises a bottom plate horizontally supported in the reaction tube and connected so as to be vertically slidable within the reaction tube.
Inventors
- 👤 Masahiko Hirose
- 👤 Katsutoshi Nishida
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 19:43
CPC Classifications
C; C09; C09C; C09C3/00; C09C3/04; C09C3/048; B; B01; B01J; B01J19/00; B01J19/08; B01J19/12; B01J19/122; B01J19/126; C01; C01B; C01B21/00; C01B21/06; C01B21/068; C01B21/0685; H; H05; H05B; H05B6/00; H05B6/64; H05B6/80; B01J2219/00; B01J2219/08; B01J2219/0894; C01P; C01P2002/00; C01P2002/70; C01P2002/80; C01P2002/82; Y; Y02; Y02P; Y02P20/00; Y02P20/10
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
170 words
An apparatus for treating powdery materials utilizing microwave plasma, comprising means for generating a microwave, a waveguide connected with said microwave generating means, a reaction vessel disposed through said waveguide, means for supplying said reaction vessel with a powdery material to be treated, means for supplying said reaction vessel with a reaction gas, and means for exhausting said reaction vessel; wherein said reaction vessel comprises a vertically elongated vessel having an upper area air tightly connected to said exhaustion means and a bottom area disposed in said waveguide so that a plasma generating area is formed at the bottom area, said vessel having a central axis and being disposed such that said central axis is oriented substantially in the direction of gravity; and said reaction gas supplying means includes a gas introducing pipe having an outlet located adjacent said bottom area, and including a movable plate positioned such that said powdery material is supported in said bottom area whereby said powdery material is blown up and agitated by the plasma.
Claim 2
Independent Claim
170 words
An apparatus for treating powdery materials utilizing microwave plasma, comprising means for generating a microwave, a waveguide connected with said microwave generating means, a reaction vessel disposed through said waveguide, means for supplying said reaction vessel with a powdery material to be treated, means for supplying said reaction vessel with a reaction gas, and means for exhausting said reaction vessel; wherein said reaction vessel comprises a vertically elongated vessel having an upper area air tightly connected to said exhaustion means and a bottom area disposed in said waveguide so that a plasma generating area is formed at the bottom area, said vessel having a central axis and being disposed such that said central axis is oriented substantially in the direction of gravity; and said reaction gas supplying means includes a gas introducing pipe having an outlet located adjacent said bottom area, and including a movable plate positioned such that said powdery material is supported in said bottom area whereby said powdery material is blown up and agitated by the plasma.
Claim 3
Dependent Claim
56 words
An apparatus according to claim 1, wherein said reaction vessel comprises a reaction tube disposed substantially vertically therein and a bottom plate horizontally supported in said reaction tube, said bottom plate being vertically slidable within said reaction tube with substantially no clearance between the side of the plate and the inner wall of the reaction tube.
Claim 4
Dependent Claim
18 words
An apparatus according to claim 2, wherein said bottom plate is a disc made of quartz or graphite.
Claim 5
Dependent Claim
26 words
An apparatus according to claim 2, wherein the reaction tube is further provided at a bottom end portion thereof with means for collecting treated powdery materials.
Claim 6
Dependent Claim
29 words
An apparatus according to claim 4, wherein the bottom plate is vertically slidable between a lower portion of the plasma generating area and the treated powdery materials collecting means.
Claim 7
Independent Claim
154 words
An apparatus for treating powdery materials utilizing a microwave plasma, comprising: means for generating microwave energy; a wave guide connected to said microwave generating means; a reaction vessel disposed through said wave guide, said reaction vessel being vertically oriented and having inlets for receiving a powdery material to be treated and a reaction gas, said reaction vessel further including a portion containing means for supporting powdery material in said wave guide, said supporting means comprising a movable plate positioned such that said powdery material is supported in said wave guide whereby said powdery material is blown up by the plasma and automatically agitated in the plasma reaction area resulting in a uniform reaction, and a powdery material outlet; means for supplying one of said reaction vessel inlets with a powdery material to be treated; means for supplying another of said reaction vessel inlets with a reaction gas; and means for exhausting said reaction vessel.
Claim 8
Independent Claim
154 words
An apparatus for treating powdery materials utilizing a microwave plasma, comprising: means for generating microwave energy; a wave guide connected to said microwave generating means; a reaction vessel disposed through said wave guide, said reaction vessel being vertically oriented and having inlets for receiving a powdery material to be treated and a reaction gas, said reaction vessel further including a portion containing means for supporting powdery material in said wave guide, said supporting means comprising a movable plate positioned such that said powdery material is supported in said wave guide whereby said powdery material is blown up by the plasma and automatically agitated in the plasma reaction area resulting in a uniform reaction, and a powdery material outlet; means for supplying one of said reaction vessel inlets with a powdery material to be treated; means for supplying another of said reaction vessel inlets with a reaction gas; and means for exhausting said reaction vessel.
Claim 9
Independent Claim
172 words
An apparatus for treating powdery materials utilizing microwave plasma, comprising means for generating a microwave, a waveguide connected with said microwave generating means, a reaction vessel disposed through said waveguide, means for supplying said reaction vessel with a powdery material to be treated, means for supplying said reaction vessel with a reaction gas, and means for exhausting said reaction vessel; wherein said reaction vessel comprises a vertically elongated vessel having an upper area air tightly connected to said exhaustion means and a bottom area disposed in said waveguide so that a plasma generating area is formed at the bottom area, said vessel having a central axis and being disposed such that said central axis is oriented substantially in the direction of gravity; and said reaction gas supplying means includes a gas introducing pipe having an outlet located adjacent said bottom area, and including a means for causing said powdery material to be supported in said waveguide in said bottom area whereby said powdery material is blown up and agitated by the plasma.
Claim 10
Independent Claim
172 words
An apparatus for treating powdery materials utilizing microwave plasma, comprising means for generating a microwave, a waveguide connected with said microwave generating means, a reaction vessel disposed through said waveguide, means for supplying said reaction vessel with a powdery material to be treated, means for supplying said reaction vessel with a reaction gas, and means for exhausting said reaction vessel; wherein said reaction vessel comprises a vertically elongated vessel having an upper area air tightly connected to said exhaustion means and a bottom area disposed in said waveguide so that a plasma generating area is formed at the bottom area, said vessel having a central axis and being disposed such that said central axis is oriented substantially in the direction of gravity; and said reaction gas supplying means includes a gas introducing pipe having an outlet located adjacent said bottom area, and including a means for causing said powdery material to be supported in said waveguide in said bottom area whereby said powdery material is blown up and agitated by the plasma.
References Cited (Backward Citations)
US3937917A
Cited
US3834038A
Cited
FR2272032A1
Cited
DE2623423A1
Cited
DE2632194A1
Cited
US4065369A
Cited
US4153527A
Cited
US4090055A
Cited
US4207452A
Cited
JPS5416480A
Cited
DE2837594A1
Cited
US4339326A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-12-26 | 1987-06-27 | 1987-12-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-12-26 | 1991-06-27 | 1991-12-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-12-26 | 1995-06-27 | 1995-12-27 | $7700.00 | Window Closed / Lapsed |