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US4329385A Expired / Lapsed US ⏱️ 0.0 years remaining

Texturing polymer surfaces by transfer casting

Assignee: National Aeronautics and Space Administration
•
Filing: 1980-12-19
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Granted: 1982-05-11
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Expires: 2000-12-19
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Abstract

Abstract This invention is concerned with fabricating textured surfaces on polymers without altering their surface chemistries. A surface of a fluorocarbon polymer 10 is exposed to a beam 12 of ions from a source 14 to texture it. The polymer 18 which is to be surface-roughened is then cast over the textured surface 20 of the fluorocarbon polymer. After curing, the cast polymer is peeled off the textured fluorocarbon polymer, and the peeled off surface 22 has a negative replica of the textured surface 20. The microscopic surface texture provides large surface areas for adhesive bonding. In cardiovascular prosthesis applications the surfaces are relied on for the development of a thin adherent well nourished thrombus.

Inventors

  • 👤 Bruce A. Banks
  • 👤 Albert J. Weigand
  • 👤 James S. Sovey

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 10:06
CPC Classifications
B; B29; B29C; B29C59/00; B29C59/16; A; A61; A61F; A61F2/00; A61F2/0077; B29C39/00; B29C39/02; B29C39/026; B29D; B29D7/00; B29D7/01; B29C35/00; B29C35/02; B29C35/08; B29C35/0866; B29C2035/0872; B29K; B29K2023/00; B29K2027/00; B29K2027/12; B29K2075/00; B29K2083/00; B29K2827/00; B29K2827/12; B29L; B29L2031/00; B29L2031/753; B29L2031/7532; B29L2031/7534; Y; Y10; Y10T; Y10T428/00; Y10T428/24; Y10T428/24355

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 128 words
A method for texturing the surfaces of a polymer without altering the chemistry of the same comprising the steps of placing a fluorocarbon polymer in a vacuum environment of about 4×10 -5 torr, exposing at least one surface of said fluorocarbon polymer to a neutralized beam of ions having an energy between about 200 eV and 2000 eV and an ion beam current density between 0.5 mA/cm 2 and 1.0 mA/cm 2 to texture the same, removing said fluorocarbon polymer from said vacuum environment, casting a polymer over said textured surface of said fluorocarbon polymer and curing the same, and separating said cast and cured polymer from said fluorocarbon polymer whereby the surface of said polymer has a negative replica of said textured surface of said fluorocarbon polymer.
Claim 2
Independent Claim 128 words
A method for texturing the surfaces of a polymer without altering the chemistry of the same comprising the steps of placing a fluorocarbon polymer in a vacuum environment of about 4×10 -5 torr, exposing at least one surface of said fluorocarbon polymer to a neutralized beam of ions having an energy between about 200 eV and 2000 eV and an ion beam current density between 0.5 mA/cm 2 and 1.0 mA/cm 2 to texture the same, removing said fluorocarbon polymer from said vacuum environment, casting a polymer over said textured surface of said fluorocarbon polymer and curing the same, and separating said cast and cured polymer from said fluorocarbon polymer whereby the surface of said polymer has a negative replica of said textured surface of said fluorocarbon polymer.
Claim 3
Dependent Claim 57 words
A method of texturing the surface of a polymer as claimed in claim 1 including providing a source of argon ions in said vacuum environment, and positioning said fluorocarbon polymer in the beam of argon ions at a location of about 20 centimeters from said source, said at least one surface being substantially normal to said beam.
Claim 4
Dependent Claim 28 words
A method of texturing the surface of a polymer as claimed in claim 2 wherein the argon ion beam is substantially uniform over said at least one surface.
Claim 5
Dependent Claim 24 words
A method of texturing the surface of a polymer as claimed in claim 1 wherein the fluorocarbon polymer is first sputtered onto a substrate.
Claim 6
Dependent Claim 29 words
A method of texturing the surface of a polymer as claimed in claim 1 wherein said polymer is selected from the group consisting of silicone rubbers, polyurethanes, and polyolefins.
Claim 7
Dependent Claim 34 words
A method of texturing the surface of a polymer as claimed in claim 1 including the step of applying a release agent to said textured surface prior to casting said polymer over the same.
Claim 8
Dependent Claim 11 words
A polymer article textured according to the process of claim 1.

References Cited (Backward Citations)

US2876187A Cited
US2928131A Cited
US3274088A Cited
US3752731A Cited
US3761338A Cited
US4064030A Cited
US4114983A Cited
US4199650A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-05-10 1985-11-09 1986-05-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-05-10 1989-11-09 1990-05-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-05-10 1993-11-09 1994-05-11 $7700.00 Window Closed / Lapsed

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