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US4282267A Expired / Lapsed US ⏱️ 0.0 years remaining

Methods and apparatus for generating plasmas

Assignee: AT&T Inc
•
Filing: 1980-03-05
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Granted: 1981-08-04
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Expires: 2000-03-05
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Abstract

Abstract An RF-excited radial-flow, cylindrical plasma reactor (10) includes a toroidal waveguide (17) of rectangular cross-section connected to a microwave source (21). One of the reactive species (37) is flowed through the waveguide and pre-ionized, thus, permitting independent control over the activation of both reactive species.

Inventors

  • 👤 Birol Kuyel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 13:31
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/44; C23C16/50; C23C16/517; B; B01; B01J; B01J19/00; B01J19/08; B01J19/12; B01J19/122; B01J19/126; H; H05; H05H; H05H1/00; H05H1/24; H05H1/46; B01J2219/00; B01J2219/08; B01J2219/0894

Claims Analysis

Total Claims: 28
Claim 1
Independent Claim 92 words
A method of separately activating at least two potentially reactive species to form a reactive plasma when combined, each of said potentially reactive species having a different activation level, said method comprising the steps of: (a) forming a non-reactive plasma so as to create therein an activated species of at least one of said potentially reactive species; (b) separately activating the other of said potentially reactive species having the higher activation level; and (c) flowing the activated species having the higher activation level into said non-reactive plasma to create a reactive plasma.
Claim 2
Independent Claim 92 words
A method of separately activating at least two potentially reactive species to form a reactive plasma when combined, each of said potentially reactive species having a different activation level, said method comprising the steps of: (a) forming a non-reactive plasma so as to create therein an activated species of at least one of said potentially reactive species; (b) separately activating the other of said potentially reactive species having the higher activation level; and (c) flowing the activated species having the higher activation level into said non-reactive plasma to create a reactive plasma.
Claim 3
Dependent Claim 36 words
The method according to claim 1 wherein said forming a non-reactive plasma step comprises: combining an inert carrier with said at least one potentially reactive species; and then ionizing said combination to form said non-reactive plasma.
Claim 4
Dependent Claim 26 words
The method according to claim 1 wherein said forming a non-reactive plasma step comprises: subjecting said at least one potentially reactive species to an electric field.
Claim 5
Dependent Claim 21 words
The method according to claim 2 wherein said forming a non-reactive plasma step comprises: subjecting said combination to an electric field.
Claim 6
Independent Claim 29 words
The method according to claims 1 or 2 wherein said separately activating step comprises: passing a beam of microwave radiation through said potentially reactive species to form a plasma.
Claim 7
Independent Claim 29 words
The method according to claims 3 or 4 wherein said separately activating step comprises: passing a beam of microwave radiation through said potentially reactive species to form a plasma.
Claim 8
Dependent Claim 51 words
The method according to claim 1 including the further step of: selectively controlling the energy supplied (1) to form a non-reactive plasma, and (2) to separately activate the other of said reactive species having the higher activation level, thereby to control the relative concentrations of activated species in said reactive plasma.
Claim 9
Dependent Claim 50 words
The method according to claim 2 including the further step of: selectively controlling the energy supplied (1) to ionize said combination, and (2) to separately activate the other of said reactive species having the higher activation level, thereby to control the relative concentrations of activated species in said reactive plasma.
Claim 10
Independent Claim 66 words
The method according to claims 1, 3 or 7 wherein said at least one potentially reactive species comprises SiH 4 , the other of said potentially reactive species having the higher activation level comprises NH 3 , and said method comprises the further step of: exposing a workpiece to said reactive plasma, whereby said plasma deposits a layer of Si 3 N 4 onto said workpiece.
Claim 11
Dependent Claim 23 words
The method according to claim 9 including the further step of: heating said workpiece to a temperature in excess of approximately 200° C.
Claim 12
Dependent Claim 26 words
The method according to claim 9 wherein said separately activating step comprises: passing a beam of microwave radiation through the other of said potentially reactive species.
Claim 13
Independent Claim 72 words
The method according to claims 2, 4 or 8 wherein said at least one potentially reactive species comprises SiH 4 , said inert carrier comprises Ar, the other of said potentially reactive species having the higher activation level comprises NH 3 , and said method comprises the further step of: exposing a workpiece to said reactive plasma whereby said reactive plasma deposits a layer of Si 3 N 4 onto said workpiece.
Claim 14
Dependent Claim 20 words
The method according to claim 12 wherein said workpiece is heated to a temperature in excess of approximately 200° C.
Claim 15
Dependent Claim 26 words
The method according to claim 12 wherein said separately activating step comprises: passing a beam of microwave radiation through the other of said potentially reactive species.
Claim 16
Independent Claim 60 words
The method according to claims 1, 3 or 7 wherein said at least one potentially reactive species comprises O 2 , the other of said potentially reactive species having the higher activation level comprises CF 4 , and said method comprises the further step of: exposing a workpiece to said reactive plasma whereby said workpiece is etched by said plasma.
Claim 17
Dependent Claim 26 words
The method according to claim 15 wherein said separately activating step comprises: passing a beam of microwave radiation through the other of said potentially reactive species.
Claim 18
Dependent Claim 91 words
Apparatus for separately activating at least two potentially reactive species to form a reactive plasma when combined, each of said potentially reactive species having a different activation level, said apparatus comprising: means for forming a non-reactive plasma so as to create therein an activated species of at least one of said potentially reactive species; means for separately activating the other of said potentially reactive species having the higher activation level; and means for flowing the activated species having the higher activation level into said non-reactive plasma to create a reactive plasma.
Claim 19
Dependent Claim 91 words
Apparatus for separately activating at least two potentially reactive species to form a reactive plasma when combined, each of said potentially reactive species having a different activation level, said apparatus comprising: means for forming a non-reactive plasma so as to create therein an activated species of at least one of said potentially reactive species; means for separately activating the other of said potentially reactive species having the higher activation level; and means for flowing the activated species having the higher activation level into said non-reactive plasma to create a reactive plasma.
Claim 20
Dependent Claim 47 words
The apparatus according to claim 17 wherein said means for forming a non-reactive plasma comprises: a sealed reaction chamber; first and second spaced-apart electrodes positioned in said chamber; and means for establishing an electric field between said first and second electrodes thereby to form a non-reactive plasma.
Claim 21
Dependent Claim 107 words
Apparatus for separately activating at least two potentially reactive species to form a reactive plasma when combined, each of said potentially reactive species having a different activation level, said apparatus comprising: means for forming a non-reactive plasma so as to create therein an activated species of at least one of said potentially reactive species; means for separately activating the other of said potentially reactive species having the higher activation level, said separately activating means further comprising: a waveguide positioned within said apparatus, said reactive species having the higher activation level flowing through said waveguide; and a source of a beam of microwave energy connected to said waveguide.
Claim 22
Dependent Claim 107 words
Apparatus for separately activating at least two potentially reactive species to form a reactive plasma when combined, each of said potentially reactive species having a different activation level, said apparatus comprising: means for forming a non-reactive plasma so as to create therein an activated species of at least one of said potentially reactive species; means for separately activating the other of said potentially reactive species having the higher activation level, said separately activating means further comprising: a waveguide positioned within said apparatus, said reactive species having the higher activation level flowing through said waveguide; and a source of a beam of microwave energy connected to said waveguide.
Claim 23
Dependent Claim 46 words
The apparatus according to claim 19 wherein said reaction chamber is cylindrical in shape, said first and second electrodes are disc-shaped and are coaxially positioned within said chamber, and said waveguide comprises a toroid of rectangular cross-section coaxial to and aligned with said first disc-shaped electrode.
Claim 24
Dependent Claim 31 words
The apparatus according to claim 20 further comprising: means, intermediate said source of microwave energy and said waveguide for passing microwave energy therethrough but for maintaining the vacuum within said chamber.
Claim 25
Dependent Claim 39 words
The apparatus according to claim 21 wherein said means for applying an electric field comprises: a source of radio frequency energy connected across said first and second electrodes; and impedance-matching means intermediate said radio frequency source and said electrodes.
Claim 26
Dependent Claim 28 words
The apparatus according to claim 22 wherein said waveguide includes a plurality of circumferentially disposed apertures to permit the flow of activated reactive species out of said waveguide.
Claim 27
Dependent Claim 35 words
The apparatus according to claim 23 further comprising: at least one ring-shaped supply pipe positioned proximate the other one of said electrodes and connected to a source of said at least one potentially reactive species.
Claim 28
Dependent Claim 15 words
The apparatus according to claim 24 including means for exhausting spent gases from said chamber.

References Cited (Backward Citations)

US3007072A Cited
US3287243A Cited
US3370198A Cited
US3916034A Cited
US3866398A Cited
US4066037A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-08-03 1985-02-02 1985-08-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-08-03 1989-02-02 1989-08-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-08-03 1993-02-02 1993-08-04 $7700.00 Window Closed / Lapsed

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