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US4174279A Expired / Lapsed US ⏱️ 0.0 years remaining

Mineral fillers

Assignee: DENVER PROCESS EQUIPMENT Ltd
•
Filing: 1978-03-29
•
Granted: 1979-11-13
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Expires: 1998-03-29
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Abstract

Abstract In a method of dewatering by pressure filtration an aqueous suspension of a clay containing a small proportion of particles having an equivalent spherical diameter smaller than 1 micron, the improvement which comprises treating the aqueous suspension of the clay, prior to dewatering by pressure filtration at a pressure in excess of 150 pounds per square inch, with a water-soluble polyelectrolyte flocculant having a high density of positive charges.

Inventors

  • 👤 Norman O. Clark
  • 👤 Thomas R. Jones

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 17:43
CPC Classifications
C; C04; C04B; C04B33/00; C04B33/02; C04B33/13

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 178 words
In a method of dewatering by pressure filtration an aqueous suspension of a kaolin clay having a particle size distribution such that it contains from 1 to 20% by weight of particles having an equivalent spherical diameter smaller than 1 micron, the improvement which comprises treating the aqueous suspension of the clay, prior to dewatering by pressure filtration at a pressure in excess of 150 pounds per square inch, with from 100 to 3000 parts by weight of a water-soluble polyelectrolyte flocculant per million parts by weight of clay, the polyelectrolyte flocculant being a polymer obtainable by copolymerising epichlorohydrin and an aliphatic secondary amine, and essentially consisting of repeating units which can be represented by the formula: ##STR4## where R and R 1 are each selected from the group consisting of hydrogen, methyl and ethyl, and X is selected from the group consisting of Cl, Br, I, HSO 4 , and CH 3 SO 4 ; and said flocculant having a molecular weight (as measured by the Ostwald viscometer method) in the range of from 50,000 to 300,000.
Claim 2
Dependent Claim 178 words
In a method of dewatering by pressure filtration an aqueous suspension of a kaolin clay having a particle size distribution such that it contains from 1 to 20% by weight of particles having an equivalent spherical diameter smaller than 1 micron, the improvement which comprises treating the aqueous suspension of the clay, prior to dewatering by pressure filtration at a pressure in excess of 150 pounds per square inch, with from 100 to 3000 parts by weight of a water-soluble polyelectrolyte flocculant per million parts by weight of clay, the polyelectrolyte flocculant being a polymer obtainable by copolymerising epichlorohydrin and an aliphatic secondary amine, and essentially consisting of repeating units which can be represented by the formula: ##STR4## where R and R 1 are each selected from the group consisting of hydrogen, methyl and ethyl, and X is selected from the group consisting of Cl, Br, I, HSO 4 , and CH 3 SO 4 ; and said flocculant having a molecular weight (as measured by the Ostwald viscometer method) in the range of from 50,000 to 300,000.
Claim 3
Dependent Claim 71 words
A method according to claim 1, wherein the clay is a white kaolin clay which contains not more than 18% by weight of particles smaller than 2 microns equivalent spherical diameter and not more than 15% by weight of particles smaller than 1 micron equivalent spherical diameter and wherein the aqueous suspension of said kaolin clay is dewatered by pressure filtration at a pressure greater than 250 pounds per square inch.
Claim 4
Dependent Claim 33 words
A method in accordance with claim 1, wherein the concentration of said water-soluble flocculant is in the range of from 500 to 2500 parts by weight per million parts by weight of clay.

References Cited (Backward Citations)

GB1240465A Cited
US3663461A Cited
US3753902A Cited
US3738945A Cited
US3855299A Cited
US4076548A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-11-12 1983-05-14 1983-11-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-11-12 1987-05-14 1987-11-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-11-12 1991-05-14 1991-11-13 $7700.00 Window Closed / Lapsed

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