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US4086125A Expired / Lapsed US ⏱️ 0.0 years remaining

Wood lamination method utilizing emulsified phenol-formaldehyde resins

Assignee: Cor Tech Research Ltd
•
Filing: 1976-12-27
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Granted: 1978-04-25
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Expires: 1996-12-27
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Abstract

Abstract A rapidly curable phenol-formaldehyde resin is provided in the form of an emulsion which has particular utility in panel board production, particularly waferboard production.

Inventors

  • 👤 Ramesh C. Vasishth
  • 👤 Pitchaiya Chandramouli

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 12:42
CPC Classifications
C; C08; C08J; C08J3/00; C08J3/02; C08J3/09; C08J3/11; B; B22; B22C; B22C1/00; B22C1/16; B22C1/20; B22C1/22; B22C1/2233; B22C1/2246; B22C1/2253; C08G; C08G8/00; C08G8/04; C08G8/08; C08G8/10; C08L; C08L97/00; C08L97/02; C09; C09J; C09J161/00; C09J161/04; C09J161/06; C08J2361/00; C08J2361/04; C08J2361/06; C08J2361/08; C08J2361/10; Y; Y10; Y10T; Y10T428/00; Y10T428/25; Y10T428/253; Y10T428/31504; Y10T428/31942; Y10T428/31949; Y10T428/31957; Y10T428/3196

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 183 words
A method of forming a panel board, which comprises: reacting formaldehyde and phenol at a mole ratio of formaldehyde to phenol greater than about 1.7:1 in an aqueous reaction medium in the presence of a metal carboxylate catalyst therefor to form a resin having a viscosity of about 1,000 to 40,000 cps at about 24° C, adding to said resin at least one strong acid in a catalyzing amount for thermosetting said resin at elevated temperature to form a room temperature-stable acid-catalyzed and mobile thermosetting phenol-formaldehyde resin capable of rapid cure at elevated temperature, emulsifying the latter resin to form a stable resin-in-water emulsion by dispersing the latter resin in water at a temperature below the curing temperature of the latter resin, applying said emulsion to a plurality of panel board-forming elements to provide a substantially even distribution of resin over part of the surfaces of said elements, assembling the coated elements, heating said resin to above its curing temperature while maintaining said coated elements in said assembled condition to adhesively join said elements together by thermoset resins, and recovering a panel board.
Claim 2
Independent Claim 183 words
A method of forming a panel board, which comprises: reacting formaldehyde and phenol at a mole ratio of formaldehyde to phenol greater than about 1.7:1 in an aqueous reaction medium in the presence of a metal carboxylate catalyst therefor to form a resin having a viscosity of about 1,000 to 40,000 cps at about 24° C, adding to said resin at least one strong acid in a catalyzing amount for thermosetting said resin at elevated temperature to form a room temperature-stable acid-catalyzed and mobile thermosetting phenol-formaldehyde resin capable of rapid cure at elevated temperature, emulsifying the latter resin to form a stable resin-in-water emulsion by dispersing the latter resin in water at a temperature below the curing temperature of the latter resin, applying said emulsion to a plurality of panel board-forming elements to provide a substantially even distribution of resin over part of the surfaces of said elements, assembling the coated elements, heating said resin to above its curing temperature while maintaining said coated elements in said assembled condition to adhesively join said elements together by thermoset resins, and recovering a panel board.
Claim 3
Dependent Claim 13 words
The method of claim 1, wherein said metal carboxylate catalyst is zinc acetate.
Claim 4
Dependent Claim 20 words
The method of claim 1, wherein said reaction is carried out wholly at a temperature of above about 90° C.
Claim 5
Dependent Claim 12 words
The method of claim 1, wherein said acid is para-toluene sulfonic acid.
Claim 6
Dependent Claim 20 words
The method of claim 4 wherein said acid is added in an amount of from 0.5 to 5% by weight.
Claim 7
Dependent Claim 20 words
The method of claim 1 wherein said panel board-forming elements are wood wafers, whereby said panel board is a waferboard.
Claim 8
Dependent Claim 32 words
The method of claim 6, wherein said emulsion is applied to the wood wafers by spraying and about 2 to about 3% by weight of resin is applied to the wood wafers.
Claim 9
Dependent Claim 20 words
The method of claim 1 wherein said panel board-forming elements are wood particles, whereby said panel board is particle board.
Claim 10
Dependent Claim 32 words
The method of claim 8 wherein said emulsion is applied to the wood particles by spraying and about 6 to about 9% by weight of resin is applied to the wood particles.
Claim 11
Dependent Claim 22 words
The method of claim 1 wherein said panel board-forming elements are wood lamina of large dimensions, whereby said panel board is plywood.

References Cited (Backward Citations)

US1976433A Cited
US2185447A Cited
US2937159A Cited
US3267053A Cited
US3422068A Cited
CA927041A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-04-24 1981-10-24 1982-04-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-04-24 1985-10-24 1986-04-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-04-24 1989-10-24 1990-04-25 $7700.00 Window Closed / Lapsed

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