US4004039A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Sweetening composition and process therefor
Assignee: General Foods Corp
•
Filing: 1975-12-08
•
Granted: 1977-01-18
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Expires: 1995-12-08
Abstract
Abstract APM is discretely dispersed throughout a matrix created by melting a fuseable mass and subdividing it to encapsulate the APM therein.
Inventors
- 👤 Myron D. Shoaf
- 👤 LaMonte D. Pischke
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-23 13:00
CPC Classifications
A; A23; A23L; A23L27/00; A23L27/30; A23L27/31; A23L27/32
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
192 words
Process for stabilizing L-aspartyl-L-phenylalanine methyl ester crystals into a particulate form adapted to be intermixed with other powderous materials and be free-flowing therewith which comprises admixing said ester crystals and a fusing and matrix-forming material selected from the group consisting of dried coffee extract, whey, low dextrose equivalent starch polymers in an intermixture with a polyol and protein extracts selected from the group consisting of gelatin and keratin, said matrix-forming material having a moisture content less than 10%, said material being molten at a temperature at or below 370° F, solidifying into a solid mass when cooled to below its melting point and retaining a thermosetting solid condition at ambient temperatures; heating the admixture of said ester crystals and said fusing and matrix-forming material to a temperature sufficient to convert said fusing and matrix-forming material into a continuous molten condition but below the melting point of the ester crystals wherein the ester crystals are discretely distributed; cooling the molten mass to fuse the same and permanently fix the ester crystals in a dispersed phase; and sub-dividing the cooled mass to a particular size thereby producing particles which encapsulate the crystals distributed therein.
Claim 2
Dependent Claim
192 words
Process for stabilizing L-aspartyl-L-phenylalanine methyl ester crystals into a particulate form adapted to be intermixed with other powderous materials and be free-flowing therewith which comprises admixing said ester crystals and a fusing and matrix-forming material selected from the group consisting of dried coffee extract, whey, low dextrose equivalent starch polymers in an intermixture with a polyol and protein extracts selected from the group consisting of gelatin and keratin, said matrix-forming material having a moisture content less than 10%, said material being molten at a temperature at or below 370° F, solidifying into a solid mass when cooled to below its melting point and retaining a thermosetting solid condition at ambient temperatures; heating the admixture of said ester crystals and said fusing and matrix-forming material to a temperature sufficient to convert said fusing and matrix-forming material into a continuous molten condition but below the melting point of the ester crystals wherein the ester crystals are discretely distributed; cooling the molten mass to fuse the same and permanently fix the ester crystals in a dispersed phase; and sub-dividing the cooled mass to a particular size thereby producing particles which encapsulate the crystals distributed therein.
Claim 3
Dependent Claim
22 words
The process of claim 1 wherein the crystals are caused to be submerged within the molten matrix by being calendered before cooling.
Claim 4
Dependent Claim
22 words
The process of claim 1 wherein said matrix-forming ingredients have a moisture content below 5% prior to conversion into a molten state.
Claim 5
Dependent Claim
13 words
The process of claim 1 wherein said matrix-forming material is dried coffee extract.
Claim 6
Dependent Claim
11 words
The process of claim 4 wherein the extract is spray dried.
Claim 7
Dependent Claim
11 words
The process of claim 1 wherein the matrix-forming material is whey.
Claim 8
Dependent Claim
11 words
The process of claim 1 wherein the matrix-forming material is gelatin.
References Cited (Backward Citations)
US3761288A
Cited
US3753739A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-01-18 | 1980-07-19 | 1981-01-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-01-18 | 1984-07-19 | 1985-01-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-01-18 | 1988-07-19 | 1989-01-18 | $7700.00 | Window Closed / Lapsed |