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US3929522A Expired / Lapsed US ⏱️ 0.0 years remaining

Process involving cooling in a static atmosphere for high permeability silicon steel comprising copper

Assignee: Allegheny Ludlum Corp
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Filing: 1974-11-18
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Granted: 1975-12-30
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Expires: 1994-11-18
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Abstract

Abstract A process for producing silicon steel having a cube-on-edge orientation and a permeability of at least 1850 (G/Oe) at 10 oersteds, which includes the steps of: preparing a melt of steel consisting essentially of, by weight, up to 0.07% carbon, from 2.60 to 4.0% silicon, from 0.03 to 0.24% manganese, from 0.01 to 0.09% of material from the group consisting of sulfur and selenium, from 0.015 to 0.04% aluminum, up to 0.02% nitrogen, from 0.1 to 0.5% copper, from 0.00045 to 0.0035% boron, balance iron; casting the steel; hot rolling the steel; annealing the steel prior to a final cold roll at a temperature of from 1400* to 2150*F; cooling the steel from a temperature below 1700*F and above 750*F to a temperature at least as low as 500*F with a liquid quenching medium or gaseous stream and from its maximum annealing temperature to the temperature below 1700*F and above 750*F at a rate which is no faster than one wherein the steel is cooled in a static atmosphere or in a continuous processing line where there is some relative motion between the atmosphere and the steel, although the only deliberate motion is that imparted to the steel; and cold rolling the steel at a reduction of at least 80%.

Inventors

  • 👤 James A Salsgiver
  • 👤 Frank A Malagari

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 10:46
CPC Classifications
C; C21; C21D; C21D8/00; C21D8/12; C21D8/1244; C21D8/1266; C22; C22C; C22C38/00; C22C38/02; C21D8/1216; C21D8/1233; C21D8/1261

Claims Analysis

Total Claims: 17
Claim 1
Independent Claim 265 words
IN A PROCESS FOR PRODUCING ELECTROMAGNETIC SILICON STEEL HAVING A CUBE-ON-EDGE ORIENTATION AND A PEREMEABILITY OF AT LEAST 1850 (G OE) AT 10 OERSTEDS, WHICH PROCESS INCLUDES THE STEPS OF: PREPARING A MELT OF SILICON STEEL; CASTING SAID STEEL; HOT ROLLING SAID STEEL INTO A HOT ROLLED BAND; SUBJECTING SAID STEEL TO AT LEAST ONE COLD ROLLING; SUBJECTING SAID STEEL TO A FINAL ANNEALING PRIOR TO THE FINAL COLD ROLLING; DECARBURIZING SAID STEEL; AND FINAL TEXTURE ANNEALING SAID STEEL; THE IMPROVEMENT COMPRISING THE STEPS OF CARRYING OUT SAID FINAL ANNEAL PRIOR TO THE FINAL COLD ROLLING AT A TEMPERATURE OF FROM 1400 TO 2150*F FOR A PERIOD OF FROM 15 SECONDS TO 2 HOURS; COOLING SAID STEEL FROM A TEMPERATURE BELOW 1700*F AND ABOVE 750*F TO A TEMPERATURE AT LEAST AS LOW AS 500*F WITH A LIQUID QUENCHING MEDIUM OR GASEOUS STREAM AND FROM ITS MAXIMUM ANNEALING TEMPERATURE TO SAID TEMPERATURE BELOW 1700*F AND ABOVE 750*F AT A RATE WHICH IS NO FASTER THAN ONE WHEREIN THE STEEL IS COOLED IN A STATIC ATMOSPHERE OR IN A CONTINUOUS PROCESSING LINE WHERE THERE IS SOME RELATIVE MOTION BETWEEN THE ATMOSPHERE AND THE STEEL, ALTHOUGH THE ONLY DELIBERATEMOTION IS THAT IMPARTED TO THE STEEL, AND SAID COOLING THE COOLED STEEL AT A REDUCTION OF ATLEAST 80%; SAID MELT CONSISTING ESSENTIALLY OF, BY WEIGHT, UP TO 0.07% CARBON, FROM 2.60 RO4.0% SILICON, FROM 0.03 TO 0.24% MANGANESE, FROM 0.01 TO 0.09% OF MATERIAL FROMTHE GROUP CONSISTING OFSULFUR ANDSELENIUM, FROM 0.015 TO0.04% ALUMINUM, UP TO 0.02% NITROGEN, FROM 0.1 TO 0.5% COPPER, FROM 0...45 TO 0.00035% BORON, BALANCE IRON.
Claim 2
Dependent Claim 265 words
IN A PROCESS FOR PRODUCING ELECTROMAGNETIC SILICON STEEL HAVING A CUBE-ON-EDGE ORIENTATION AND A PEREMEABILITY OF AT LEAST 1850 (G OE) AT 10 OERSTEDS, WHICH PROCESS INCLUDES THE STEPS OF: PREPARING A MELT OF SILICON STEEL; CASTING SAID STEEL; HOT ROLLING SAID STEEL INTO A HOT ROLLED BAND; SUBJECTING SAID STEEL TO AT LEAST ONE COLD ROLLING; SUBJECTING SAID STEEL TO A FINAL ANNEALING PRIOR TO THE FINAL COLD ROLLING; DECARBURIZING SAID STEEL; AND FINAL TEXTURE ANNEALING SAID STEEL; THE IMPROVEMENT COMPRISING THE STEPS OF CARRYING OUT SAID FINAL ANNEAL PRIOR TO THE FINAL COLD ROLLING AT A TEMPERATURE OF FROM 1400 TO 2150*F FOR A PERIOD OF FROM 15 SECONDS TO 2 HOURS; COOLING SAID STEEL FROM A TEMPERATURE BELOW 1700*F AND ABOVE 750*F TO A TEMPERATURE AT LEAST AS LOW AS 500*F WITH A LIQUID QUENCHING MEDIUM OR GASEOUS STREAM AND FROM ITS MAXIMUM ANNEALING TEMPERATURE TO SAID TEMPERATURE BELOW 1700*F AND ABOVE 750*F AT A RATE WHICH IS NO FASTER THAN ONE WHEREIN THE STEEL IS COOLED IN A STATIC ATMOSPHERE OR IN A CONTINUOUS PROCESSING LINE WHERE THERE IS SOME RELATIVE MOTION BETWEEN THE ATMOSPHERE AND THE STEEL, ALTHOUGH THE ONLY DELIBERATEMOTION IS THAT IMPARTED TO THE STEEL, AND SAID COOLING THE COOLED STEEL AT A REDUCTION OF ATLEAST 80%; SAID MELT CONSISTING ESSENTIALLY OF, BY WEIGHT, UP TO 0.07% CARBON, FROM 2.60 RO4.0% SILICON, FROM 0.03 TO 0.24% MANGANESE, FROM 0.01 TO 0.09% OF MATERIAL FROMTHE GROUP CONSISTING OFSULFUR ANDSELENIUM, FROM 0.015 TO0.04% ALUMINUM, UP TO 0.02% NITROGEN, FROM 0.1 TO 0.5% COPPER, FROM 0...45 TO 0.00035% BORON, BALANCE IRON.
Claim 3
Dependent Claim 98 words
An improvement according to claim 1, wherein said steel is cooled from a temperature below 1600*F and above 1000*F to a temperature at least as low as 500*F with a liquid quenching medium or gaseous stream and from its maximum annealing temperature to said temperature below 1600*F and above 1000*F at a rate which is no faster than one wherein the steel is is cooled in a static atmosphere or in a continuous processing line where there is some relative motion between the atmosphere and the steel, although the only deliberate motion is that imparted to the steel.
Claim 4
Dependent Claim 24 words
An improvement according to claim 1, wherein said final anneal prior to the final cold rolling is at a temperature from 1800* to 2125*F.
Claim 5
Dependent Claim 97 words
An improvement according to claim 3, wherein said steel is cOoled from a temperature below 1600*F and above 1000*F to a temperature at least as low as 500*F with a liquid quenching medium or gaseous stream and from its maximum annealing temperature to said temperature below 1600*F and above 1000*F at a rate which is no faster than one wherein the steel is cooled in a static atmosphere or in a continuous processing line where there is some relative motion between the atmosphere and the steel, although the only deliberate motion is that imparted to the steel.
Claim 6
Dependent Claim 32 words
An improvement according to claim 1, wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700*F and above 750*F with a gaseous stream.
Claim 7
Dependent Claim 33 words
An improvement according to claim 1, wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700*F and above 750*F with a liquid quenching medium.
Claim 8
Dependent Claim 20 words
An improvement according to claim 1, wherein said steel is air cooled to said temperature below 1700*F and above 750*F.
Claim 9
Dependent Claim 32 words
An improvement according to claim 3, wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700*F and above 750*F with a gaseous stream.
Claim 10
Dependent Claim 33 words
An improvement according to claim 3, wherein said steel is cooled to a temperature at least as low as 500*F from a temperature below 1700*F and above 750*F with a liquid quenching medium.
Claim 11
Dependent Claim 20 words
An improvement according to claim 3, wherein said steel is air cooled to said temperature below 1700*F and above 750*F.
Claim 12
Dependent Claim 25 words
An improvement according to claim 1, wherein said final anneal prior to the final cold rolling is carried out subsequent to an initial cold rolling.
Claim 13
Dependent Claim 65 words
An improvement according to claim 1, wherein said steel consists essentially of, by weight, from 0.02 to 0.07% carbon, from 2.65 to 3.25% silicon, from 0.05 to 0.20% manganese, from 0.02 to 0.09% of material from the group consisting of sulfur and selenium, from 0.015 to 0.04% aluminum, from 0.0030 to 0.0090% nitrogen, from 0.1 to 0.4% copper, from 0.0005 to 0.0025% boron, balance iron.
Claim 14
Dependent Claim 14 words
An improvement according to claim 12, wherein said steel has at least 0.0007% boron.
Claim 15
Dependent Claim 20 words
An improvement according to claim 1, wherein the cooled steel is cold rolled at a reduction of at least 85%.
Claim 16
Dependent Claim 20 words
An improvement according to claim 3, wherein the cooled steel is cold rolled at a reduction of at least 85%.
Claim 17
Dependent Claim 23 words
An improvement according to claim 1, wherein said final anneal prior to the final cold rolling is applied to a hot rolled band.

References Cited (Backward Citations)

US3287184A Cited
US3632456A Cited
US3671337A Cited
US3764406A Cited
US3770517A Cited
US3855018A Cited
US3855018B1 Cited
US3855019A Cited
US3855020A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-12-29 1979-06-30 1979-12-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-12-29 1983-06-30 1983-12-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-12-29 1987-06-30 1987-12-30 $7700.00 Window Closed / Lapsed

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