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US3857682A Expired / Lapsed US ⏱️ 0.0 years remaining

High temperature resistive and dry lubricated film surfaces

Assignee: White Engineering Corp
•
Filing: 1973-02-07
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Granted: 1974-12-31
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Expires: 1993-02-07
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Abstract

Abstract A high particulate energy level deposited composite film build up is presented with a layer atomically bonded to the substrate carrier material and graduated hardness material film layers including refractory material. The substrate carrier material has a relatively high thermal conductivity factor relative to refractory material used in a film layer. A dry lube reaction overcoating film or one of other dry lube films are also deposited over hard dense film surfaces for lubricity between moving parts in a heated environment.

Inventors

  • 👤 G White

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 18:54
CPC Classifications
F; F16; F16J; F16J10/00; C; C23; C23C; C23C14/00; C23C14/22; C23C14/24; C23C14/32; C23C24/00; C30; C30B; C30B23/00; C30B23/02; C30B23/08; F01; F01C; F01C19/00; F01C19/02; F01C19/04; F01D; F01D5/00; F01D5/12; F01D5/28; F01D5/288; F05; F05D; F05D2300/00; F05D2300/20; F05D2300/22; F05D2300/224; Y; Y02; Y02T; Y02T50/00; Y02T50/60; Y10; Y10S; Y10S428/00; Y10S428/922; Y10S428/923; Y10S428/924; Y10S428/926; Y10T; Y10T428/00; Y10T428/12; Y10T428/12458; Y10T428/12493; Y10T428/12535; Y10T428/12542; Y10T428/12549; Y10T428/12576; Y10T428/12583; Y10T428/1259; Y10T428/12736; Y10T428/12743; Y10T428/1275

Claims Analysis

Total Claims: 28
Claim 1
Independent Claim 93 words
A HIGH TEMPERATURE RESISTIVE FILM BLUID-UP DEPOSITED ON SUBSTRATE MATERIAL, WITH A PLURALITY OF FILM MATERIALS WITH FILM MATERIAL ATOMS MECHANICALLY DRIVEN INTO UNDERLYING MATERIAL ATOMIC LATTICE IN PHASE ZONES OF ATOMS OF ADJOINING MATERIALS THROUGH USE OF HIGH PARTICULATE ENERGY LEVEL FILM MATERIAL DEPOSITION ION PLATING PROCESS, WITH AT LEAST TWO OF THE MATERIALS OF THE MATERIALS OF SAID SUBSTRATE AND SAID PLURALITY OF FILM MATERIALS BEING METAL BASED MATERIALS; AND WITH AT LEAST ONE FILM MATERIAL A HARDENED REFRACTORY MATERIAL FILM DEPOSITED BY A HIGH PARTICULATE ENERGY LEVEL ION PLANTING PROCESS.
Claim 2
Dependent Claim 93 words
A HIGH TEMPERATURE RESISTIVE FILM BLUID-UP DEPOSITED ON SUBSTRATE MATERIAL, WITH A PLURALITY OF FILM MATERIALS WITH FILM MATERIAL ATOMS MECHANICALLY DRIVEN INTO UNDERLYING MATERIAL ATOMIC LATTICE IN PHASE ZONES OF ATOMS OF ADJOINING MATERIALS THROUGH USE OF HIGH PARTICULATE ENERGY LEVEL FILM MATERIAL DEPOSITION ION PLATING PROCESS, WITH AT LEAST TWO OF THE MATERIALS OF THE MATERIALS OF SAID SUBSTRATE AND SAID PLURALITY OF FILM MATERIALS BEING METAL BASED MATERIALS; AND WITH AT LEAST ONE FILM MATERIAL A HARDENED REFRACTORY MATERIAL FILM DEPOSITED BY A HIGH PARTICULATE ENERGY LEVEL ION PLANTING PROCESS.
Claim 3
Dependent Claim 56 words
The high temperature resistive film build-up of claim 1, wherein said film build-up is a graduated hardness material film build-up from the substrate material progressively in higher hardness steps upward through refractory material filming. 3. The high temperature resistive film build-up of claim 2, wherein the maximum hardness ratio step is approximately 2 1/2 to 1.
Claim 4
Dependent Claim 43 words
The high temperature resistive film build-up of claim 2, wherein the substrate material is aluminum coated with sequential layers of nickle, chromium, chromium oxide, and titanium carbide with Knoop hardness values running successively approximately 200 to 557 to 920 to 1,600 to 2,300.
Claim 5
Dependent Claim 30 words
The high temperature resistive film build-up of claim 2, wherein said film build-up is provided with an overcoating of dry lubricant material from among the class including gold and silver.
Claim 6
Dependent Claim 20 words
The high temperature resistive film build-up of claim 2, including an oxide material overcoating with inherently good dry lubricity qualities.
Claim 7
Dependent Claim 28 words
The high temperature resistive film build-up of claim 2, including an overcoating of dry lubricant film material that is a layered lattice inorganic compound such as molybdenum disulphide.
Claim 8
Dependent Claim 15 words
The high temperature resistive film build-up of claim 2, including an overcoating of Titanium Nitride.
Claim 9
Dependent Claim 22 words
The high temperature resistive film build-up of claim 2, wherein said film build-up is on a heat engine high temperature internal surface.
Claim 10
Dependent Claim 18 words
The high temperature resistive film build-up of claim 2, wherein said film build-up is an epitaxial film build-up.
Claim 11
Dependent Claim 20 words
The high temperature resistive film build up of claim 10, wherein said film build-up is at least one mil thick.
Claim 12
Dependent Claim 53 words
The high temperature resistive film build-up of claim 2, wherein said refractory material deposited in filming is deposited to a thickness limiting heat through flow, with operational hot wall design temperatures, from said hot wall as a high temperature surface to said substrate material within non-destructive heat conveying capability of the substrate material.
Claim 13
Dependent Claim 47 words
The high temperature resistive film build-up of claim 2, wherein said film build-up is applied on internal combustion chamber walling in a heat engine having an increased high temperature operational limit with said film build-up; and an increased temperature differential range of operation and increased operational efficiency.
Claim 14
Dependent Claim 38 words
The high temperature resistive film build-up of claim 13, with said heat engine having sliding contact high temperature surfaces with said film build-ups; and with outer dry lubricant material films deposited over said sliding contact high temperature surfaces.
Claim 15
Dependent Claim 49 words
The high temperature resistive film build-up of claim 2, wherein a layer of distributive material having a relatively high heat conductivity factor, such as not to be considered a refractory material, is included in said film build-up as a heat conductor minimizing hot spots in the film build up.
Claim 16
Dependent Claim 20 words
The high temperature resistive film build-up of claim 1, including an overcoating film of dry lubricant material deposited by sputtering.
Claim 17
Dependent Claim 24 words
The high temperature resistive film build-up of claim 1, including an overcoating film of dry lubricant material deposited by an ion deposition plating process.
Claim 18
Dependent Claim 53 words
The high temperature resistive film build-up of claim 1, with a film of chromium over underlying material; and a film of gold over the film of chromium in at least a two layer structure with both the chromium and gold films being the plating results of high particulate energy level ion plating processes.
Claim 19
Dependent Claim 42 words
The high temperature resistive film build-up of claim 1, wherein the plurality of film materials include successively from the base substrate material, an adhesion material film, a distributive material film, an insulation refractory material film, and a dry lubricity material overcoating film.
Claim 20
Dependent Claim 30 words
The high temperature resistive film buil-up of claim 19, wherein chromium is the adhesion material film, chromium oxide the distributive material film, and hafnium oxide the insulation refractory material film.
Claim 21
Dependent Claim 29 words
The high temperature resistive film build-up of claim 1, wherein the plurality of film materials includes adjacent layers of chromium and chromium oxide each over approximately 1,000 angstroms thick.
Claim 22
Dependent Claim 28 words
The high temperature resistive film build-up of claim 1, wherein the plurality of film materials include successively from the base substrate material hafnium, hafnium oxide and molybdenum disulphide.
Claim 23
Dependent Claim 27 words
The high temperature resistive film build-up of claim 1, wherein the plurality of film materials include successively from the base substrate material titanium, titanium nitride and gold.
Claim 24
Dependent Claim 28 words
The high temperature resistive film build-up of claim 1, wherein the plurality of film materials include successively from the base substrate material titanium, titanium carbide and titanium nitride.
Claim 25
Dependent Claim 28 words
The high temperature resistive film build-up of claim 1, wherein the plurality of film materials include successively from the base substrate material titanium, titanium carbide and titanium oxide.
Claim 26
Dependent Claim 27 words
The high temperature resistive film build-up of claim 1, with the film build-up deposited on internal high temperature component surface areas of a rotary internal combustion engine.
Claim 27
Dependent Claim 32 words
The high temperature resistive film build-up of claim 1, with said film build-up deposited on high temperature internal cylinder walls and high temperature operational components of a reciprocating piston and cylinder structures.
Claim 28
Dependent Claim 22 words
The high temperature resistive film build-up of claim 1, with said film build-up deposited on jet engine hot gas operational turbine blades.

References Cited (Backward Citations)

US3075279A Cited
US3031331A Cited
US3091548A Cited
US3117846A Cited
US3454375A Cited
US3640689A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-12-30 1978-07-01 1978-12-31 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-12-30 1982-07-01 1982-12-31 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-12-30 1986-07-01 1986-12-31 $7700.00 Window Closed / Lapsed

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