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Method for preparing insoluble,cross-linked organic hydrogels comprising copolymers of glycol monoesters with diesters

Assignee: Czech Academy of Sciences
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Filing: 1968-07-23
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Granted: 1971-09-21
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Expires: 1988-07-23
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Abstract

Abstract Insoluble hydrogels are prepared by cross-linking linear or branched soluble copolymers of glycol methacrylates or glycol acrylates with glycol dimethacrylates or glycol diacrylates, preferably in presence of glycol acrylate or glycol methacrylate monomers which may contain the respective diester, and preferably also in presence of initiators liberating free radicals, and in presence of solvents having the interaction parameter Chi . Soluble glycol methacrylate or acrylate polymers can be used in form of fine solid particles and the cross-linking may be aided by heating till to about 150* C.

Inventors

  • 👤 Vladimir Stoy
  • 👤 Richard Chromecek
  • 👤 Zdenek Tuzar
  • 👤 Miroslav Stol
  • 👤 Karel Kliment
  • 👤 Jaroslava Otoupalova
  • 👤 Miloslav Bohdanecky

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 10:26
CPC Classifications
C; C08; C08F; C08F20/00; C08F20/02; C08F20/10; C08F20/26; C08F20/28; C08F265/00; C08F265/04; Y; Y10; Y10S; Y10S623/00; Y10S623/924

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 26 words
Method as set forth in claim 1, wherein the final step of cross-linking is carried out by heating to temperatures ranging from 85 to 200* C.
Claim 2
Dependent Claim 38 words
Method as set forth in claim 1, wherein the final step of cross-linking is carried out in presence of an added major amount relative to said monomers of a comonomer capable of copolymerization with the said soluble copolymer.
Claim 3
Dependent Claim 34 words
Method as set forth in claim 1, wherein the final step of cross-linking is carried out in presence of solvents, having the interaction parameter with respect to the polymer thus formed higher than 0.5.
Claim 4
Dependent Claim 24 words
Method as set forth in claim 1, wherein the final step of cross-linking is carried out in presence of polymerization initiators liberating free radicals.
Claim 5
Dependent Claim 21 words
Method as set forth in claim 1, wherein the final step of cross-linking is carried out by irradiating with ionizing rays.

References Cited (Backward Citations)

No citation records indexed.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-09-20 1975-03-22 1975-09-21 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-09-20 1979-03-22 1979-09-21 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-09-20 1983-03-22 1983-09-21 $7700.00 Window Closed / Lapsed

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