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US3597450A Expired / Lapsed US ⏱️ 0.0 years remaining

Preparation of glycolide polymerizable into polyglycolic acid of consistently high molecular weight

Assignee: Wyeth Holdings LLC
•
Filing: 1969-11-05
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Granted: 1971-08-03
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Expires: 1989-11-05
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Abstract

Abstract WHEREAS RECRYSTALLIZATION ALONE, OR SUBLIMATION ALONE, OF IMPURE GLYCOLIDE DOES NOT, IN THE MAJORITY OF CASES, RENDER GLYCOLIDE SUFFICIENTLY PURE TO PERMIT ITS POLYMERIZATION INTO POLYGLYCOLIC ACID OF THE HIGH MOLECULAR WEIGHT VARIETY REQUIRED FOR USE AS AN ABSORBABLE SURGICAL SUTURE OR LIGATURE, IT IS SURPRISINGLY FOUND THAT WHEN IMPURE GLYCOLIDE IS SUBJECTED TO THE DUAL SEQUENTIAL STEPS OF RECRYSTALLIZATION AND SUBLIMATION, THE GLYCOLIDE PRODUCED IS SUFFICIENTLY PURE TO PRODUCE CONSISTENTLY HIGH MOLECULAR WEIGHT POLYGLYCOLIC ACID, PROVIDED THE SUBLIMATION STEP FOLLOWS THE RECRYSTALLIZATION STEP.

Inventors

  • 👤 Edward Emil Schmitt
  • 👤 Rocco Albert Polistina
  • 👤 Martin Epstein
  • 👤 David Anthony Deprospero

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 18:57
CPC Classifications
C; C08; C08G; C08G63/00; C08G63/02; C08G63/06; C08G63/08; C07; C07D; C07D319/00; C07D319/10; C07D319/12

Claims Analysis

Total Claims: 0
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References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-08-02 1975-02-01 1975-08-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-08-02 1979-02-01 1979-08-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-08-02 1983-02-01 1983-08-03 $7700.00 Window Closed / Lapsed

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