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EP0108601A2 Expired / Lapsed EP ⏱️ 0.0 years remaining

Polypropylene membranes

Assignee: Akzo NV
•
Filing: 1983-11-01
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Granted: —
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Expires: 2003-11-01
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Abstract

Abstract There is disclosed a substantially skinless microporous polypropylene membrane characterized by having (a) a bubble point in the range of from 25 to 50 psi; (b) a thickness in the range of from 3 to 7 mils; (c) a nitrogen flow rate of at least 0.5 liters per square centimeter-minute; (d) a burst strength of at least 10 psi; and (e) an S value of about 15, or less. There is also disclosed a method of preparing a microporous polypropylene membrane comprising heating a mixture of about 30 percent polypropylene and about 70 percent, N,N-bis(2-hydroxyethyl)tallowamine, by weight, to a temperature and for a time sufficient to form a homogeneous solution, casting or extruding said solution at a thickness in the range of from 3 to 7 mils, onto a chill roll maintained at a temperature in the range of from 50 to 80°C, allowing the solution to solidify on the chill roll to form a solid sheet, removing the solid sheet from the chill roll and removing at least a substantial portion of the liquid from the sheet to form the microporous polypropylene membrane.

Inventors

  • 👤 Gunter H. Vitzthum
  • 👤 Michael A. Davis

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-10-23 05:01
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/28; B; B01; B01D; B01D67/00; B01D67/0002; B01D67/0023; B01D67/003; B01D69/00; B01D69/02; B01D71/00; B01D71/06; B01D71/26; B01D71/262; C08J2201/00; C08J2201/02; C08J2201/03; C08J2201/04; C08J2201/052; C08J2201/054; C08J2201/0542; C08J2323/00; C08J2323/02; C08J2323/10; C08J2323/12; Y; Y10; Y10T; Y10T428/00; Y10T428/249921; Y10T428/249953; Y10T428/249978; Y10T428/249979

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 66 words
A substantially skinless microporous polypropylene membrane characterized by having (a) a bubble point in the range of from 25 to 50 psi; (b) a thickness in the range of from 3 to 7 mils; (c) a nitrogen flow rate of at least 0.5 liters per square centimeter-minute; (d) a burst strength of at least 10 psi; and (e) an S value of about 15, or less.
Claim 2
Dependent Claim 66 words
A substantially skinless microporous polypropylene membrane characterized by having (a) a bubble point in the range of from 25 to 50 psi; (b) a thickness in the range of from 3 to 7 mils; (c) a nitrogen flow rate of at least 0.5 liters per square centimeter-minute; (d) a burst strength of at least 10 psi; and (e) an S value of about 15, or less.
Claim 3
Dependent Claim 20 words
A membrane as claimed in claim 1 which has a skin throughout no more than 10 percent of its cross-section.
Claim 4
Dependent Claim 23 words
A membrane as claimed in claim 1 or .claim 2 which has a thickness in the range of from 3.5 to 4.0 mils.
Claim 5
Dependent Claim 23 words
A membrane as claimed in any one of the preceding claims having a flow rate of at least 0.7 liters per square centimeter-minute.
Claim 6
Dependent Claim 43 words
A membrane as claimed in claim 4 having a skin throughout less than 5 percent of its cross-section, having a thickness in the range of from 3.5 to 4.0 mils, and having a sharpness value in the range of from 8 to 14.
Claim 7
Independent Claim 112 words
A method of preparing a substantially skinless microporous polypropylene membrane comprising heating a mixture of about 30 percent polypropylene and about 70 percent, N,N-bis(2-hydroxyethyl)tallowamine, by weight, to a temperature and for a time sufficient to form a homogeneous solution, castingor extruding the solution at a thickness in the range of from 3 to 7 mils, onto a chill roll maintained at a temperature in the range of from 50 to 80°C, allowing the solution to solidify on the chill roll to form a solid sheet, removing the solid sheet from the chill roll and removing at least a substantial portion of the liquid from the sheet to form the microporous polypropylene membrane.
Claim 8
Independent Claim 112 words
A method of preparing a substantially skinless microporous polypropylene membrane comprising heating a mixture of about 30 percent polypropylene and about 70 percent, N,N-bis(2-hydroxyethyl)tallowamine, by weight, to a temperature and for a time sufficient to form a homogeneous solution, castingor extruding the solution at a thickness in the range of from 3 to 7 mils, onto a chill roll maintained at a temperature in the range of from 50 to 80°C, allowing the solution to solidify on the chill roll to form a solid sheet, removing the solid sheet from the chill roll and removing at least a substantial portion of the liquid from the sheet to form the microporous polypropylene membrane.
Claim 9
Dependent Claim 21 words
A method as claimed in claim 6 wherein the solution is cast at a thickness of from 3.5 to 4 mils.
Claim 10
Dependent Claim 18 words
A method as claimed in claim 6 or claim 7 wherein the chill roll temperature is about 60°C.
Claim 11
Independent Claim 19 words
A method as claimed in any one of claims 6 to 8 wherein the liquid is removed with isopropanol..
Claim 12
Independent Claim 40 words
A method as claimed in any one of claims 6 to 9 wherein a wiper bar is used on the chill roll prior to the location at which the homogeneous solution is cast or : extruded onto the chill roll.

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